Technology Process of [22R,(+)]-1α-Acetyloxy-3β-[(β-D-glucopyranosyl)oxy]-20,22-dihydroxyergosta-5,24-diene-26-oic acid 26,22-lactone
There total 2 articles about [22R,(+)]-1α-Acetyloxy-3β-[(β-D-glucopyranosyl)oxy]-20,22-dihydroxyergosta-5,24-diene-26-oic acid 26,22-lactone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride; sodium tetrahydroborate; sodium periodate;
Yield given. Multistep reaction;
1.) MeOH, H2O, 16 h, 4 deg C, 12 h, room temp.; 2.) MeOH, 1 h, room temp.; 3.) 24 h, room temp.;
DOI:10.1016/S0031-9422(00)80538-5
- Guidance literature:
-
With
hydrogenchloride; sodium tetrahydroborate; sodium periodate;
Yield given. Multistep reaction;
1.) MeOH, H2O, 16 h, 4 deg C, 12 h, room temp.; 2.) MeOH, 1 h, room temp.; 3.) 24 h, room temp.;
DOI:10.1016/S0031-9422(00)80538-5