3,4-dichlorobenzenebutanal

Base Information

Chemical Name:3,4-dichlorobenzenebutanal
CAS No.:1310094-84-8
Molecular Formula:C₁₀H₁₀Cl₂O
Molecular Weight:217.095
Hs Code.:

Synonyms:3,4-dichlorobenzenebutanal

Suppliers and Price of 3,4-dichlorobenzenebutanal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 3,4-dichlorobenzenebutanal

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,4-dichlorobenzenebutanal

There total 6 articles about 3,4-dichlorobenzenebutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1343315-52-5
4-(3,4-dichlorophenyl)butan-1-ol

: 1310094-84-8
4-(3,4-dichlorophenyl)butanal

Guidance literature:: With silica gel; pyridinium chlorochromate; In dichloromethane; for 1h;

Reference yield:

: 39960-05-9
3-(3 ,4-dichlorophenyl)propan-1-ol

: 1310094-84-8
4-(3,4-dichlorophenyl)butanal

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanesulfonyl chloride / pyridine / 3 h / 20 °C

1.2: 72 h / 0 - 20 °C

2.1: water; sodium hydroxide / ethanol / 3 h / Reflux

3.1: borane-THF / tetrahydrofuran / 0 - 20 °C

4.1: silica gel; pyridinium chlorochromate / dichloromethane / 1 h

With borane-THF; water; silica gel; methanesulfonyl chloride; pyridinium chlorochromate; sodium hydroxide; In tetrahydrofuran; pyridine; ethanol; dichloromethane;

Reference yield:

: 25173-68-6
3(3,4-dichlorophenyl)propanoic acid

: 1310094-84-8
4-(3,4-dichlorophenyl)butanal

Guidance literature:: Multi-step reaction with 5 steps

1.1: borane-THF / tetrahydrofuran / 12 h / 0 °C

2.1: methanesulfonyl chloride / pyridine / 3 h / 20 °C

2.2: 72 h / 0 - 20 °C

3.1: water; sodium hydroxide / ethanol / 3 h / Reflux

4.1: borane-THF / tetrahydrofuran / 0 - 20 °C

5.1: silica gel; pyridinium chlorochromate / dichloromethane / 1 h

With borane-THF; water; silica gel; methanesulfonyl chloride; pyridinium chlorochromate; sodium hydroxide; In tetrahydrofuran; pyridine; ethanol; dichloromethane;