Ethanone, 1-[2-(1-propenyl)-1-cyclohexen-1-yl]-, (Z)- (9CI)

Base Information

Chemical Name:Ethanone, 1-[2-(1-propenyl)-1-cyclohexen-1-yl]-, (Z)- (9CI)
CAS No.:132079-96-0
Molecular Formula:C11H16O
Molecular Weight:164.24414
Hs Code.:
Mol file:132079-96-0.mol

Synonyms:Ethanone, 1-[2-(1-propenyl)-1-cyclohexen-1-yl]-, (Z)- (9CI)

Suppliers and Price of Ethanone, 1-[2-(1-propenyl)-1-cyclohexen-1-yl]-, (Z)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Ethanone, 1-[2-(1-propenyl)-1-cyclohexen-1-yl]-, (Z)- (9CI)

Chemical Property:

PSA：17.07000
LogP:3.02210

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-[2-(1-propenyl)-1-cyclohexen-1-yl]-, (Z)- (9CI)

There total 3 articles about Ethanone, 1-[2-(1-propenyl)-1-cyclohexen-1-yl]-, (Z)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66680-84-0,66680-85-1,105494-65-3
(Z)-1-propenyltributyltin

: 132079-92-6
2-<(Methanesulfonyl)oxy>-1-acetylcyclohexene

: 132079-96-0
2-((Z)-Prop-1-en-1-yl)-1-acetylcyclohexene

: 132079-94-8
2-((E)-Prop-1-en-1-yl)-1-acetylcyclohexene

Guidance literature:: With lithium bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 80 ℃; for 36h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00004a028

Reference yield:

: 24850-33-7
allyltributylstanane

: 132079-92-6
2-<(Methanesulfonyl)oxy>-1-acetylcyclohexene

: 132079-97-1
1-(2-Allyl-cyclohex-1-enyl)-ethanone

: 132079-96-0
2-((Z)-Prop-1-en-1-yl)-1-acetylcyclohexene

: 132079-94-8
2-((E)-Prop-1-en-1-yl)-1-acetylcyclohexene

Guidance literature:: With lithium bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 80 ℃; for 36h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00004a028

Reference yield:

: 874-23-7,125117-37-5
2-acetylcyclohexanone

: 132079-96-0
2-((Z)-Prop-1-en-1-yl)-1-acetylcyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / NEt₃ / 1,2-dimethoxy-ethane / 12 h / Ambient temperature

2: LiBr / Pd(PPh₃)4 / tetrahydrofuran / 36 h / 80 °C

With triethylamine; lithium bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,2-dimethoxyethane;
DOI:10.1021/jo00004a028