4-(2-BROMOPHENYL)-1-METHYL-1H-PYRROLE-3-CARBOXYLIC ACID ETHYL ESTER

Base Information

Chemical Name:4-(2-BROMOPHENYL)-1-METHYL-1H-PYRROLE-3-CARBOXYLIC ACID ETHYL ESTER
CAS No.:938164-26-2
Molecular Formula:C14H14BrNO2
Molecular Weight:308.175
Hs Code.:
Mol file:938164-26-2.mol

Synonyms:4-(2-BROMOPHENYL)-1-METHYL-1H-PYRROLE-3-CARBOXYLIC ACID ETHYL ESTER

Suppliers and Price of 4-(2-BROMOPHENYL)-1-METHYL-1H-PYRROLE-3-CARBOXYLIC ACID ETHYL ESTER

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2-BROMOPHENYL)-1-METHYL-1H-PYRROLE-3-CARBOXYLIC ACID ETHYL ESTER

Chemical Property:

Melting Point:104 - 106 °C (ethyl acetate)
PSA：31.23000
LogP:3.63130

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of 4-(2-BROMOPHENYL)-1-METHYL-1H-PYRROLE-3-CARBOXYLIC ACID ETHYL ESTER

There total 2 articles about 4-(2-BROMOPHENYL)-1-METHYL-1H-PYRROLE-3-CARBOXYLIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 938164-56-8
4-(2-bromo-phenyl)-1H-pyrrole-3-carboxylic acid ethyl ester

: 74-88-4
methyl iodide

: 938164-26-2
4-(2-bromo-phenyl)-1-methyl-1H-pyrrole-3-carboxylic acid ethyl ester

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/ol070475w

Reference yield:

: 99134-25-5
(E:Z)-3-(2-bromo-phenyl)-acrylic acid ethyl ester

: 938164-26-2
4-(2-bromo-phenyl)-1-methyl-1H-pyrrole-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / sodium hydride / diethyl ether; various solvent(s); dimethylformamide / 3 h

2: 88 percent / sodium hydride / dimethylformamide; various solvent(s) / 2 h / 20 °C

With sodium hydride; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ol070475w