5,6-DIHYDROXY-2-PHENYL-PYRIMIDINE-4-CARBOXYLIC ACID METHYL ESTER

Base Information

• Chemical Name: 5,6-DIHYDROXY-2-PHENYL-PYRIMIDINE-4-CARBOXYLIC ACID METHYL ESTER
• CAS No.: 62222-36-0
• Molecular Formula: C12H10N2O4
• Molecular Weight: 246.222
• Hs Code.: 2933599090
• Mol file: 62222-36-0.mol

Synonyms:5,6-DIHYDROXY-2-PHENYL-PYRIMIDINE-4-CARBOXYLIC ACID METHYL ESTER;methyl 5,6-dihydroxy-2-phenylpyrimidine-4-carboxylate

Chemical Property of 5,6-DIHYDROXY-2-PHENYL-PYRIMIDINE-4-CARBOXYLIC ACID METHYL ESTER

Chemical Property:

• PSA: 92.54000
• LogP: 1.34140

Purity/Quality:

97% ^*data from raw suppliers

5,6-Dihydroxy-2-phenyl-pyrimidine-4-carboxylicacidmethylester 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5,6-DIHYDROXY-2-PHENYL-PYRIMIDINE-4-CARBOXYLIC ACID METHYL ESTER

There total 15 articles about 5,6-DIHYDROXY-2-PHENYL-PYRIMIDINE-4-CARBOXYLIC ACID METHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C13H14N2O5 (1422555-43-8,33229-29-7) → methyl 5-hydroxy-6-oxo-2-phenyl-1,6-dihydropyrimidine-4-carboxylate (62222-36-0)

Guidance literature:

With 1,10-phenanthroline copper(II) dichloride; In 2-methyltetrahydrofuran; at 60 ℃; Sealed tube; Inert atmosphere;

DOI:10.1002/anie.201201720

Reference yield: 50.0%

(E)-2-(Benzimidoyl-aminooxy)-but-2-enedioic acid dimethyl ester (33229-29-7) → methyl 5-hydroxy-6-oxo-2-phenyl-1,6-dihydropyrimidine-4-carboxylate (62222-36-0)

Guidance literature:

In o-xylene; at 20 - 182 ℃; for 0.0236111h; microwave irradiation;

DOI:10.1016/j.tetlet.2005.12.057

Reference yield:

C13H14N2O5 (33229-29-7) → methyl 5-hydroxy-6-oxo-2-phenyl-1,6-dihydropyrimidine-4-carboxylate (62222-36-0)

Guidance literature:

In 5,5-dimethyl-1,3-cyclohexadiene; at 20 - 90 ℃; for 30h; Reflux; Inert atmosphere;

DOI:10.1016/j.bmc.2014.07.036

upstream raw materials:

N-hydroxybenzenecarboximidamide

dimethyl acetylenedicarboxylate

(E)-2-(Benzimidoyl-aminooxy)-but-2-enedioic acid dimethyl ester

N-hydroxyl-benzamidine

Downstream raw materials:

5,6-dihydroxy-2-phenyl-pyrimidine-4-carboxylic acid

N-(cyclohexylmethyl)-5,6-dihydroxy-2-phenylpyrimidine-4-carboxamide

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