Ethyl 2-chloro-6-formylbenzoate

Base Information

Chemical Name:Ethyl 2-chloro-6-formylbenzoate
CAS No.:1049677-64-6
Molecular Formula:C10H9ClO3
Molecular Weight:212.633
Hs Code.:2918300090
DSSTox Substance ID:DTXSID00705321
Nikkaji Number:J3.100.713E
Wikidata:Q82638150
Mol file:1049677-64-6.mol

Synonyms:ethyl 2-chloro-6-formylbenzoate;1049677-64-6;Ethyl 2-chloro-6-formyl-benzoate;2-chloro-6-formyl-benzoic acid ethyl ester;ethyl2-chloro-6-formylbenzoate;SCHEMBL17981647;DTXSID00705321;ZRB67764;MFCD09859805;SB30380;AS-37688;2-chloro-6-formylbenzoic acid ethyl ester;2-Formyl-6-chlorobenzoic acid ethyl ester;CS-0107310;FT-0720086

Suppliers and Price of Ethyl 2-chloro-6-formylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Ethyl2-Chloro-6-formyl-benzoate
50mg
$ 45.00

J&W Pharmlab
2-Chloro-6-formyl-benzoicacidethylester 96%
5g
$ 600.00

J&W Pharmlab
2-Chloro-6-formyl-benzoicacidethylester 96%
1g
$ 200.00

J&W Pharmlab
2-Chloro-6-formyl-benzoicacidethylester 96%
500mg
$ 150.00

Crysdot
Ethyl2-chloro-6-formylbenzoate 95+%
5g
$ 841.00

Chemenu
ethyl2-chloro-6-formylbenzoate 95%
5g
$ 794.00

American Custom Chemicals Corporation
ETHYL 2-CHLORO-6-FORMYL-BENZOATE 95.00%
1G
$ 1089.05

Total 7 raw suppliers

Chemical Property of Ethyl 2-chloro-6-formylbenzoate

Chemical Property:

Boiling Point:323.0±27.0 °C(Predicted)
PSA：43.37000
Density:1.269±0.06 g/cm3(Predicted)
LogP:2.32920
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:212.0240218
Heavy Atom Count:14
Complexity:217

Purity/Quality:

97% ^*data from raw suppliers

Ethyl2-Chloro-6-formyl-benzoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=C(C=CC=C1Cl)C=O

Technology Process of Ethyl 2-chloro-6-formylbenzoate

There total 3 articles about Ethyl 2-chloro-6-formylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1400692-87-6
ethyl 2-chloro-6-(1,3-dioxolan-2-yl)benzoate

: 1049677-64-6
ethyl 2-chloro-6-formylbenzoate

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; for 4h; Reflux;
DOI:10.1055/s-0031-1289784

Reference yield:

: 64380-53-6
2-(3-chlorophenyl)-1,3-dioxolane

: 1049677-64-6
ethyl 2-chloro-6-formylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 °C / Inert atmosphere

1.2: -78 - -20 °C / Inert atmosphere

2.1: hydrogenchloride / tetrahydrofuran; water / 4 h / Reflux

With hydrogenchloride; n-butyllithium; In tetrahydrofuran; hexane; water;
DOI:10.1055/s-0031-1289784

Reference yield:

: 587-04-2
m-Chlorobenzaldehyde

: 1049677-64-6
ethyl 2-chloro-6-formylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / toluene / 14 h / Reflux; Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 °C / Inert atmosphere

2.2: -78 - -20 °C / Inert atmosphere

3.1: hydrogenchloride / tetrahydrofuran; water / 4 h / Reflux

With hydrogenchloride; n-butyllithium; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; water; toluene;
DOI:10.1055/s-0031-1289784