N-Methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Base Information

Chemical Name:N-Methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
CAS No.:1197171-76-8
Molecular Formula:C14H20BNO3
Molecular Weight:261.129
Hs Code.:2931900090
DSSTox Substance ID:DTXSID90682213
Wikidata:Q82606519
Mol file:1197171-76-8.mol

Synonyms:1197171-76-8;N-Methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide;3-(N-Methylaminocarbonyl)phenylboronic acid, pinacol ester;N-methyl-3-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide;3-(N-Methylaminocarbonyl)phenylboronic acid pinacol ester;3-(N-METHYLAMINOCARBONYL)PHENYLBORONIC ACID,PINACOL ESTER;N-Methyl-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)benzamide;SCHEMBL1284689;DTXSID90682213;YKVCWFPOJAXHGE-UHFFFAOYSA-N;MFCD17015821;ZB1412;AKOS022168253;AS-2801;SB17894;CS-0008228;FT-0766032;H10931;EN300-7370184;A927348;Benzamide, N-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-

Suppliers and Price of N-Methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-(N-Methylaminocarbonyl)phenylboronicAcidPinacolEster
100mg
$ 75.00

TRC
3-(N-Methylaminocarbonyl)phenylboronicAcidPinacolEster
50mg
$ 60.00

SynQuest Laboratories
N-Methyl-3-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
5 g
$ 493.00

SynQuest Laboratories
N-Methyl-3-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
1 g
$ 103.00

Matrix Scientific
N-Methyl-3-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide >95%
1g
$ 166.00

Matrix Scientific
N-Methyl-3-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide >95%
500mg
$ 123.00

Matrix Scientific
N-Methyl-3-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide >95%
5g
$ 498.00

Crysdot
N-Methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide 95+%
10g
$ 377.00

Apolloscientific
N-Methyl-3-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
1g
$ 93.00

Apolloscientific
N-Methyl-3-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide
5g
$ 447.00

Total 19 raw suppliers

Chemical Property of N-Methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Chemical Property:

Storage Temp.:Room temperature.
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:261.1536237
Heavy Atom Count:19
Complexity:341

Purity/Quality:

97% ^*data from raw suppliers

3-(N-Methylaminocarbonyl)phenylboronicAcidPinacolEster ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OC(C(O1)(C)C)(C)C)C2=CC(=CC=C2)C(=O)NC

Technology Process of N-Methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

There total 8 articles about N-Methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 49834-22-2
3-bromo-N-methylbenzamide

: 73183-34-3
bis(pinacol)diborane

: 1197171-76-8
N-methyl-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzamide

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 80 ℃; for 1h; Inert atmosphere;

Reference yield: 94.0%

: 88070-48-8
N-methylbenzamide

: 73183-34-3
bis(pinacol)diborane

: 214360-57-3
N-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-benzamide

: 1197171-76-8
N-methyl-3-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzamide

: N-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzamide

Guidance literature:: With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; N-(2,3-dimethyl-1H-indol-7-yl)-[2,2'-bipyridine]-5-carboxamide; In tetrahydrofuran; at 50 ℃; for 24h; regioselective reaction; Inert atmosphere; Glovebox;
DOI:10.1002/anie.201907366