Technology Process of 4,9-Dibromo-2,7-bis(2-butyloctyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone
There total 2 articles about 4,9-Dibromo-2,7-bis(2-butyloctyl)benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetraone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid dianhydride;
With
acetic acid;
at 20 ℃;
for 0.5h;
Inert atmosphere;
2-butyloctan-1-amine;
at 120 ℃;
for 3h;
Temperature;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dibromoisocyanuric acid; fuming sulphuric acid / 27 h / 20 - 90 °C
2.1: acetic acid / 0.5 h / 20 °C / Inert atmosphere
2.2: 3 h / 120 °C
With
fuming sulphuric acid; acetic acid; dibromoisocyanuric acid;
