4-Benzyloxy-thiobenzamide

Base Information

• Chemical Name: 4-Benzyloxy-thiobenzamide
• CAS No.: 161975-22-0
• Molecular Formula: C14H13NOS
• Molecular Weight: 243.329
• DSSTox Substance ID: DTXSID10428913
• Wikidata: Q82241762
• Mol file: 161975-22-0.mol

Synonyms:4-BENZYLOXY-THIOBENZAMIDE;161975-22-0;4-(BENZYLOXY)BENZOTHIOAMIDE;4-phenylmethoxybenzenecarbothioamide;4-benzyloxythiobenzamide;MFCD06738327;Benzenecarbothioamide, 4-(phenylmethoxy)-;SCHEMBL6890765;DTXSID10428913;AKOS000133520;AB26900;BS-15503;CS-0156175;4-(BENZYLOXY)BENZENE-1-CARBOTHIOAMIDE;4-(Benzyloxy)benzenecarbothioamide, AldrichCPR;Y13465;EN300-1865705;A883034

Chemical Property of 4-Benzyloxy-thiobenzamide

Chemical Property:

• PSA: 67.34000
• LogP: 3.60010
• Storage Temp.: Sealed in dry,Room Temperature
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 243.07178521
• Heavy Atom Count: 17
• Complexity: 243

Purity/Quality:

97% ^*data from raw suppliers

4-(Benzyloxy)benzenecarbothioamide Aldrich ^*data from reagent suppliers

Safty Information:

• Statements: 43
• Safety Statements: 36/37

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)COC2=CC=C(C=C2)C(=S)N

Technology Process of 4-Benzyloxy-thiobenzamide

There total 4 articles about 4-Benzyloxy-thiobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-benzyloxybenzonitrile (52805-36-4) → 4-(benzyloxy) benzothioamide (161975-22-0)

Guidance literature:

With diammonium sulfide; 1,6-bis(3-methylimidazolium-1-yl)hexane dichloride; at 70 ℃; for 0.833333h;

DOI:10.1007/BF03246065

Reference yield: 62.0%

4-benzyloxybenzaldehyde oxime (76193-67-4) → 4-(benzyloxy) benzothioamide (161975-22-0)

Guidance literature:

With ammonium sulfide; trichlorotitanium(IV) trifluoromethanesulfonate; 1-n-butyl-3-methylimidazolim bromide; at 80 ℃; for 4.3h; chemoselective reaction; Ionic liquid;

DOI:10.1016/j.tetlet.2008.09.084

Reference yield:

4-cyanophenol (767-00-0) → 4-(benzyloxy) benzothioamide (161975-22-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone / Reflux

2: sodium hydrogen sulfide; magnesium chloride / N,N-dimethyl-formamide / 20 °C

With sodium hydrogen sulfide; potassium carbonate; magnesium chloride; In N,N-dimethyl-formamide; acetone;

DOI:10.1016/j.bmcl.2012.10.022

upstream raw materials:

4-benzyloxybenzaldehyde oxime

4-benzyloxybenzonitrile

4-cyanophenol

benzyl bromide

Downstream raw materials:

C₂₅H₂₂ClNO₂S

C₃₂H₃₇ClN₂O₂S

C₃₃H₃₇ClN₂O₂S

C₃₂H₃₅ClN₂O₂S

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 161975-22-0 4-BENZYLOXY-THIOBENZAMIDE

Send

Send

Metric Ton KG G Pound L ML

Send

Send