2-(1-pyrrolidinyl)acetohydrazide(SALTDATA: 2HCl)

Base Information

• Chemical Name: 2-(1-pyrrolidinyl)acetohydrazide(SALTDATA: 2HCl)
• CAS No.: 7171-96-2
• Molecular Formula: C6H14ClN3O
• Molecular Weight: 143.189
• Hs Code.: 2933990090
• Mol file: 7171-96-2.mol

Synonyms:2-(1-pyrrolidinyl)acetohydrazide(SALTDATA: 2HCl);Pyrrolidin-1-yl-acetic acid hydrazide

Chemical Property of 2-(1-pyrrolidinyl)acetohydrazide(SALTDATA: 2HCl)

Chemical Property:

• PSA: 58.36000
• LogP: 0.90320

Purity/Quality:

98%+ ^*data from raw suppliers

Pyrrolidin-1-yl-aceticacidhydrazide 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(1-pyrrolidinyl)acetohydrazide(SALTDATA: 2HCl)

There total 2 articles about 2-(1-pyrrolidinyl)acetohydrazide(SALTDATA: 2HCl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.1%

ethyl 2-(pyrrolidin-1-yl) acetate (22041-19-6) → 2-(pyrrolidin-1-yl)acetyl hydrazine (7171-96-2)

Guidance literature:

With hydrazine hydrate; In ethanol; at 80 ℃; for 12h;

Reference yield:

methyl 2-(pyrrolidin-1-yl)acetate (22041-18-5) → 2-(pyrrolidin-1-yl)acetyl hydrazine (7171-96-2)

Guidance literature:

With hydrazine hydrate; In methanol; Reflux;

Reference yield: 71.3%

2-(pyrrolidin-1-yl)acetyl hydrazine (7171-96-2) + (E)-N'-(1-(4-methoxyphenyl)-7-oxo-6-(4-(2-oxopiperidin-1-yl)phenyl)-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridin-3-yl)-N,N-dimethylformimidamide → 1-(4-methoxyphenyl)-6-(4-(2-oxopiperidin-1-yl)phenyl)-3-(3-(pyrrolidin-1-ylmethyl)-4H-1,2,4-triazol-4-yl)-1,4,5,6-tetrahydro-7H-pyrazolo[3,4-c]pyridin-7-one

Guidance literature:

With acetic acid; at 80 ℃; for 2h;

DOI:10.1016/j.bmc.2017.03.055

upstream raw materials:

methyl 2-(pyrrolidin-1-yl)acetate

ethyl 2-(pyrrolidin-1-yl) acetate

Downstream raw materials:

5-(pyrrolidin-1-ylmethyl)-1,3,4-oxadiazole-2(3H)-thione

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