3-(4-CHLOROBENZOYL)THIOPHENE

Base Information

• Chemical Name: 3-(4-CHLOROBENZOYL)THIOPHENE
• CAS No.: 896618-56-7
• Molecular Formula: C11H7ClOS
• Molecular Weight: 222.69
• Hs Code.: 2934999090
• Mol file: 896618-56-7.mol

Synonyms:3-(4-CHLOROBENZOYL)THIOPHENE

Chemical Property of 3-(4-CHLOROBENZOYL)THIOPHENE

Chemical Property:

• Vapor Pressure: 7.79E-05mmHg at 25°C
• Boiling Point: 341.9°C at 760 mmHg
• Flash Point: 160.6°C
• PSA: 45.31000
• Density: 1.317g/cm³
• LogP: 3.63250

Purity/Quality:

95% ^*data from raw suppliers

(4-chlorophenyl)(thiophen-3-yl)methanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 3-(4-CHLOROBENZOYL)THIOPHENE

There total 4 articles about 3-(4-CHLOROBENZOYL)THIOPHENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

tri(3-thienyl)aluminium (1446424-90-3) + 4-chlorobenzaldehyde (104-88-1) → (4-chlorophenyl)(thiophen-3-yl)methanone (896618-56-7)

Guidance literature:

tri(3-thienyl)aluminium; 4-chlorobenzaldehyde; With 3,3-dimethyl-butan-2-one; at 20 ℃; for 3h; Cooling with ice;

With trifluoroacetic acid; at 20 ℃; for 48h;

DOI:10.1039/c3ob40642c

Reference yield: 65.0%

thiophen-3-ylmanganese(II) chloride + 4-chloro-benzoyl chloride (122-01-0) → (4-chlorophenyl)(thiophen-3-yl)methanone (896618-56-7)

Guidance literature:

In tetrahydrofuran; at 10 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c4ob01235f

Reference yield: 58.0%

C4H3BrMgS*C2H6OZn*LiCl + 4-chlorobenzaldehyde (104-88-1) → (4-chlorophenyl)(thiophen-3-yl)methanone (896618-56-7)

Guidance literature:

With pivalaldehyde; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/aoc.4462

upstream raw materials:

5,5-dimethyl-2-(thiophen-3-yl)-1,3,2-dioxaborinane

4-chlorobenzaldehyde

tri(3-thienyl)aluminium

4-chloro-benzoyl chloride

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