4-BROMO-2-FLUOROPHENYL CYCLOPROPYL KETONE

Base Information

• Chemical Name: 4-BROMO-2-FLUOROPHENYL CYCLOPROPYL KETONE
• CAS No.: 898790-15-3
• Molecular Formula: C10H8BrFO
• Molecular Weight: 243.075
• Mol file: 898790-15-3.mol

Synonyms:4-BROMO-2-FLUOROPHENYL CYCLOPROPYL KETONE

Chemical Property of 4-BROMO-2-FLUOROPHENYL CYCLOPROPYL KETONE

Chemical Property:

• Vapor Pressure: 0.000902mmHg at 25°C
• Boiling Point: 303.9°C at 760 mmHg
• Flash Point: 137.6°C
• PSA: 17.07000
• Density: 1.613g/cm³
• LogP: 3.18090

Purity/Quality:

≥95% ^*data from raw suppliers

(4-Bromo-2-fluorophenyl)(cyclopropyl)methanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-BROMO-2-FLUOROPHENYL CYCLOPROPYL KETONE

There total 4 articles about 4-BROMO-2-FLUOROPHENYL CYCLOPROPYL KETONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

1-(4-bromo-2-fluorophenyl)-1-cyclopropylmethanol → (4-bromo-2-fluorophenyl)(cyclopropyl)methanone (898790-15-3)

Guidance literature:

With manganese(IV) oxide; In dichloromethane; at 50 ℃; for 18h;

Reference yield: 36.0%

cyclopropylmagnesium bromide (23719-80-4) + 4-bromo-2-fluorobenzaldehyde (57848-46-1) → (4-bromo-2-fluorophenyl)(cyclopropyl)methanone (898790-15-3) + 1-(4-bromo-2-fluorophenyl)-1-cyclopropylmethanol

Guidance literature:

In tetrahydrofuran; at -78 - 12 ℃; for 17h; Inert atmosphere;

Reference yield:

cyclopropyl bromide (4333-56-6,130561-87-4) + 4-bromo-2-fluorobenzaldehyde (57848-46-1) → (4-bromo-2-fluorophenyl)(cyclopropyl)methanone (898790-15-3)

Guidance literature:

cyclopropyl bromide; With magnesium; In tetrahydrofuran; at 20 ℃; for 1h;

4-bromo-2-fluorobenzaldehyde; In tetrahydrofuran; at 20 ℃; for 48h;

upstream raw materials:

cyclopropyl bromide

4-bromo-2-fluorobenzaldehyde

cyclopropylmagnesium bromide

Downstream raw materials:

6-bromo-3-cyclopropyl-1H-indazole

C₂HF₃O₂*C₂₁H₂₀F₃N₃O₃S

C₃₇H₃₆F₃N₃O₅S

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