Methanesulfonato2-Di-t-butylphosphino-2'-(N,N-dimethylamino)biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II)

Base Information

• Chemical Name: Methanesulfonato2-Di-t-butylphosphino-2'-(N,N-dimethylamino)biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II)
• CAS No.: 1445085-92-6
• Molecular Weight: 711.21
• Mol file: 1445085-92-6.mol

Synonyms:Methanesulfonato2-Di-t-butylphosphino-2'-(N,N-dimethylamino)biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II)

Chemical Property of Methanesulfonato2-Di-t-butylphosphino-2'-(N,N-dimethylamino)biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II)

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

Methanesulfonato[2-(di-t-butylphosphino)-2'-(N,N-dimethylamino)-1,1'-biphenyl](2'-amino-1,1'-biphenyl-2-yl)palladium(II) dichloromethane adduct, min. 98% [t-BuDavePhos Palladacycle Gen. 3] ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: tBuDavePhos Pd G3 has been used as a precatalyst for the Synthesis of Aryl Sulfonamides via Palladium-Catalyzed Chlorosulfonylation of Arylboronic Acids. It may also be used for a variety of C-C and C-N cross-coupling reactions.

Technology Process of Methanesulfonato2-Di-t-butylphosphino-2'-(N,N-dimethylamino)biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II)

There total 3 articles about Methanesulfonato2-Di-t-butylphosphino-2'-(N,N-dimethylamino)biphenyl)(2'-amino-1,1'-biphenyl-2-yl)palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(2'-amino-1,1'-biphenyl-2-yl)methanesulfonatopalladium(II) dimer (1435520-65-2) + 2'-(di-tert-butylphosphanyl)-N,N-dimethyl-[1,1'-biphenyl]-2-amine (224311-49-3) → C22H32NP*C13H13NO3PdS (1445085-92-6)

Guidance literature:

In tetrahydrofuran; at 20 ℃;

DOI:10.1039/c2sc20903a

Reference yield:

2-phenylaniline (90-41-5) → C22H32NP*C13H13NO3PdS (1445085-92-6)

Guidance literature:

Multi-step reaction with 3 steps

1: Isopropyl acetate / 20 °C

2: toluene / 65 °C

3: tetrahydrofuran / 20 °C

In tetrahydrofuran; Isopropyl acetate; toluene;

DOI:10.1039/c2sc20903a

Reference yield:

[1,1'-biphenyl]-2-aminium methanesulfonate (1445085-50-6) → C22H32NP*C13H13NO3PdS (1445085-92-6)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 65 °C

2: tetrahydrofuran / 20 °C

In tetrahydrofuran; toluene;

DOI:10.1039/c2sc20903a

upstream raw materials:

(2'-amino-1,1'-biphenyl-2-yl)methanesulfonatopalladium(II) dimer

2'-(di-tert-butylphosphanyl)-N,N-dimethyl-[1,1'-biphenyl]-2-amine

2-phenylaniline

[1,1'-biphenyl]-2-aminium methanesulfonate

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