NAPHTHALENE (13C6)

Base Information

Chemical Name:NAPHTHALENE (13C6)
CAS No.:287399-34-2
Molecular Formula:C₁₀H₈
Molecular Weight:134.108
Hs Code.:
Mol file:287399-34-2.mol

Synonyms:NAPHTHALENE (13C6);Albocarbon-13C6;Dezodorator-13C6;Moth Flakes-13C6;NSC 37565-13C6;Tar CaMphor-13C6;White Tar-13C6

Suppliers and Price of NAPHTHALENE (13C6)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Naphthalene-13C6
2.5mg
$ 185.00

American Custom Chemicals Corporation
NAPHTHALENE-1,2,3,4,9,10-13C6 95.00%
10MG
$ 1871.10

American Custom Chemicals Corporation
NAPHTHALENE-1,2,3,4,9,10-13C6 95.00%
5MG
$ 1452.00

Total 3 raw suppliers

Chemical Property of NAPHTHALENE (13C6)

Chemical Property:

PSA：0.00000
LogP:2.83980

Purity/Quality:

99% atom 13C ^*data from raw suppliers

Naphthalene-13C6 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of NAPHTHALENE (13C6)

There total 6 articles about NAPHTHALENE (13C6) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 75-21-8,99932-75-9
oxirane

: 1262053-54-2
[1,2,3,4,4a,8a-⁽¹³⁾C₆]-2-bromonaphthalene

: 287399-34-2,287399-39-7
[1,2,3,4,4a,8a-(13)C6]naphthalene

: 1262053-56-4
[1,2,3,4,4a,8a-⁽¹³⁾C₆]naphthalen-2-ethanol

Guidance literature:: [1,2,3,4,4a,8a-⁽¹³⁾C₆]-2-bromonaphthalene; With n-butyllithium; In diethyl ether; pentane; for 0.0833333h; Inert atmosphere;

oxirane; In diethyl ether; pentane; for 0.5h; Cooling with ice; Inert atmosphere;
DOI:10.1002/jlcr.1798

Reference yield:

: C₄⁽¹³⁾C₆H₁₁BrO

: 287399-34-2,287399-39-7
[1,2,3,4,4a,8a-(13)C6]naphthalene

: 1262053-56-4
[1,2,3,4,4a,8a-⁽¹³⁾C₆]naphthalen-2-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / toluene / 1.25 h / 70 - 75 °C

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 1.25 h / 100 °C

3.1: n-butyllithium / diethyl ether; pentane / 0.08 h / Inert atmosphere

3.2: 0.5 h / Cooling with ice; Inert atmosphere

With n-butyllithium; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; diethyl ether; toluene; pentane;
DOI:10.1002/jlcr.1798

Reference yield:

: 1262053-50-8
4-(4-bromo-⁽¹³⁾C₆-phenyl)-4-oxobutanoic acid

: 287399-34-2,287399-39-7
[1,2,3,4,4a,8a-(13)C6]naphthalene

: 1262053-56-4
[1,2,3,4,4a,8a-⁽¹³⁾C₆]naphthalen-2-ethanol

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hydroxide / water; diethylene glycol / 0.5 h

1.2: 21.5 h / 20 - 180 °C / Inert atmosphere

2.1: polyphosphoric acid / 1.5 h / 90 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 1 h / 20 °C

4.1: toluene-4-sulfonic acid / toluene / 1.25 h / 70 - 75 °C

5.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 1.25 h / 100 °C

6.1: n-butyllithium / diethyl ether; pentane / 0.08 h / Inert atmosphere

6.2: 0.5 h / Cooling with ice; Inert atmosphere

With sodium tetrahydroborate; n-butyllithium; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; water; toluene; pentane; diethylene glycol; 1.2: Huang-Minlon reduction / 2.1: Friedel-Crafts acylation;
DOI:10.1002/jlcr.1798