Ethyl 2-(4-bromo-2-fluorophenyl)acetate

Base Information

• Chemical Name: Ethyl 2-(4-bromo-2-fluorophenyl)acetate
• CAS No.: 924312-09-4
• Molecular Formula: C10H10BrFO2
• Molecular Weight: 261.091
• Mol file: 924312-09-4.mol

Synonyms:Ethyl 2-(4-bromo-2-fluorophenyl)acetate;(4-Bromo-2-fluoro-phenyl)-acetic acid ethyl ester

Chemical Property of Ethyl 2-(4-bromo-2-fluorophenyl)acetate

Chemical Property:

• PSA: 26.30000
• LogP: 2.69380

Purity/Quality:

99%, ^*data from raw suppliers

Ethyl2-(4-bromo-2-fluorophenyl)acetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethyl 2-(4-bromo-2-fluorophenyl)acetate

There total 2 articles about Ethyl 2-(4-bromo-2-fluorophenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

2-(4-bromo-2-fluoro-phenyl)acetic acid (114897-92-6) + ethanol (64-17-5) → ethyl 2-(4-bromo-2-fluorophenyl)acetate (924312-09-4)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

Reference yield: 70.0%

ethanol (64-17-5) + (4-bromo-2-fluorophenyl)acetonitrile (114897-91-5) → ethyl 2-(4-bromo-2-fluorophenyl)acetate (924312-09-4)

Guidance literature:

ethanol; (4-bromo-2-fluorophenyl)acetonitrile; With hydrogenchloride; In water; for 15h; Heating / reflux;

With water; sodium hydrogencarbonate; at 0 ℃;

Reference yield: 96.0%

ethyl 2-(4-bromo-2-fluorophenyl)acetate (924312-09-4) → ethyl 2-bromo-2-(4-bromo-2-fluorophenyl)acetate (1426050-73-8)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 90 ℃; for 9h;

upstream raw materials:

ethanol

(4-bromo-2-fluorophenyl)acetonitrile

2-(4-bromo-2-fluoro-phenyl)acetic acid

Downstream raw materials:

2-(4-bromo-2-fluoro-phenyl)acetic acid

2-(4-bromo-2-fluorophenyl)-N-[(1-ethylpyrrolidin-2-yl)methyl]acetamide

ethyl 2-bromo-2-(4-bromo-2-fluorophenyl)acetate

ethyl 2-(4-bromo-2-fluorophenyl)-2-(4-ethyl-3-oxo-1-oxa-4,9-diazaspiro[5.5]undecan-9-yl)acetate

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