3-(2-bromoethyl)tetrahydrofuran(SALTDATA: FREE)

Base Information

• Chemical Name: 3-(2-bromoethyl)tetrahydrofuran(SALTDATA: FREE)
• CAS No.: 1229624-12-7
• Molecular Formula: C6H11BrO
• Molecular Weight: 179.05
• Hs Code.: 2932190090
• Mol file: 1229624-12-7.mol

Synonyms:3-(2-bromoethyl)tetrahydrofuran(SALTDATA: FREE);3-(2-bromoethyl)-tetrahydrofuran

Chemical Property of 3-(2-bromoethyl)tetrahydrofuran(SALTDATA: FREE)

Chemical Property:

• PSA: 9.23000
• LogP: 1.80790

Purity/Quality:

97% ^*data from raw suppliers

3-(2-Bromoethyl)tetrahydrofuran ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(2-bromoethyl)tetrahydrofuran(SALTDATA: FREE)

There total 3 articles about 3-(2-bromoethyl)tetrahydrofuran(SALTDATA: FREE) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanesulfonic acid 2-(tetrahydro-furan-3-yl)-ethyl ester (476415-59-5) → 3-(2-bromoethyl)tetrahydrofuran (1229624-12-7)

Guidance literature:

With lithium bromide; In acetone; for 4h; Heating / reflux;

Reference yield:

3-(2'-hydroxyethyl)tetrahydrofuran (130990-25-9) → 3-(2-bromoethyl)tetrahydrofuran (1229624-12-7)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

2: lithium bromide / acetone / 4 h / Heating / reflux

With triethylamine; lithium bromide; In dichloromethane; acetone;

Reference yield:

3-[(E/Z)-2-methoxyethenyl]tetrahydrofuran (1050494-76-2) → 3-(2-bromoethyl)tetrahydrofuran (1229624-12-7)

Guidance literature:

Multi-step reaction with 3 steps

1.1: hydrogenchloride; ethanol; water / 21 h / 20 - 50 °C

1.3: 3 h

2.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

3.1: lithium bromide / acetone / 4 h / Heating / reflux

With hydrogenchloride; ethanol; water; triethylamine; lithium bromide; In dichloromethane; acetone;

upstream raw materials:

methanesulfonic acid 2-(tetrahydro-furan-3-yl)-ethyl ester

3-(2'-hydroxyethyl)tetrahydrofuran

3-[(E/Z)-2-methoxyethenyl]tetrahydrofuran

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