4,7-Methano-1H-inden-1-ol, octahydro-, (1S,3aS,4S,7R,7aR)- (9CI)

Base Information

• Chemical Name: 4,7-Methano-1H-inden-1-ol, octahydro-, (1S,3aS,4S,7R,7aR)- (9CI)
• CAS No.: 585544-46-3
• Molecular Formula: C₁₀H₁₆O
• Molecular Weight: 152.236
• Mol file: 585544-46-3.mol

Synonyms:4,7-Methano-1H-inden-1-ol, octahydro-, (1S,3aS,4S,7R,7aR)- (9CI)

Chemical Property of 4,7-Methano-1H-inden-1-ol, octahydro-, (1S,3aS,4S,7R,7aR)- (9CI)

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

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• Pictogram(s):  
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Technology Process of 4,7-Methano-1H-inden-1-ol, octahydro-, (1S,3aS,4S,7R,7aR)- (9CI)

There total 12 articles about 4,7-Methano-1H-inden-1-ol, octahydro-, (1S,3aS,4S,7R,7aR)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

exo-tricyclo<5.2.1.02,6>decan-3-one (17364-68-0) → exo-1-hydroxy-2,3,3a,4,5,6,7,7a-octahydro-exo-4,7-methano-1H-indene (10271-47-3,82752-64-5,10271-46-2,55255-97-5,82752-63-4,585544-46-3)

Guidance literature:

With sodium tetrahydroborate; In ethanol; 1.) 0 deg C, 1 h, 2.) reflux, 2 h;

DOI:10.1021/jo00345a052

Reference yield: 84.0%

(1RS,3aRS,4RS,7SR,7aSR)-3a,4,7,7a-tetrahydro-4,7-methano-1H-inden-1-ol (24529-79-1) → endo-1-hydroxy-2,3,3a,4,5,6,7,7a-octahydro-exo-4,7-methano-1H-indene (10271-46-2,82752-63-4,10271-47-3,55255-97-5,82752-64-5,585544-46-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; under 2280 Torr;

DOI:10.1021/jo00345a052

Reference yield: 80.0%

endo-tricyclo<5.2.1.02.6>decan-3-one (17364-68-0) → 3-exo-hydroxy-endo-tricyclo<5.2.1.02,6>decane (10271-46-2,585544-46-3) + 5,6-endo-trimethylene-8-endo-norbornanol (585544-46-3)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; Heating;

DOI:10.1021/jo00350a028

upstream raw materials:

exo-endo-tricyclo[5.2.1.0^2,6]dec-4-ene-3-ol

3a,4,5,6,7,7a-hexahydro-4,7-methano-1H-indene

endo-tricyclo<5.2.1.0².⁶>decan-3-one

Tricyclo[5.2.1.0^2,6]decan-2-ol

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