4-ANISIC ACID POTASSIUM SALT

Base Information

• Chemical Name: 4-ANISIC ACID POTASSIUM SALT
• CAS No.: 52509-81-6
• Molecular Formula: C8H8 O3 . K
• Molecular Weight: 190.24
• Hs Code.: 2918990090
• Mol file: 52509-81-6.mol

Synonyms:Benzoicacid, 4-methoxy-, potassium salt (9CI); Potassium 4-methoxybenzoate; Potassiump-anisate

Chemical Property of 4-ANISIC ACID POTASSIUM SALT

Chemical Property:

• Vapor Pressure: 0.00206mmHg at 25°C
• Boiling Point: 211.6°Cat760mmHg
• Flash Point: 84.2°C
• PSA: 49.36000
• Density: 0.94g/cm³
• LogP: 0.05870

Purity/Quality:

98%Min ^*data from raw suppliers

4-ANISIC ACID POTASSIUM SALT 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-ANISIC ACID POTASSIUM SALT

There total 3 articles about 4-ANISIC ACID POTASSIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

methyl 4-methoxybenzoate (121-98-2) → potassium 4-methoxybenzoate (52509-81-6)

Guidance literature:

With Triton X-114; potassium thioacetate; at 150 ℃;

DOI:10.1016/j.tetlet.2005.11.048

Reference yield:

4-methoxybenzoic acid (100-09-4) → potassium 4-methoxybenzoate (52509-81-6)

Guidance literature:

With potassium tert-butylate; In ethanol; for 1h;

DOI:10.1002/anie.201208755

Reference yield:

4-Methoxybenzyl alcohol (105-13-5) → potassium 4-methoxybenzoate (52509-81-6)

Guidance literature:

With chloro(η⁶-p-cymene)[2-(2,6-diisopropylphenyl)-5-(1,3-diisopropyl-2,4,6-trioxohexahydropyrimidin-5-yl-κC⁵)imidazo[1,5-a]pyridin-3-ylidene-κC³]ruthenium(II); potassium hydroxide; In dichloromethane; o-xylene; at 150 ℃; Schlenk technique;

DOI:10.1021/acs.organomet.1c00458

upstream raw materials:

methyl 4-methoxybenzoate

4-methoxybenzoic acid

4-Methoxybenzyl alcohol

Downstream raw materials:

(4-methoxybenzoyloxymethyl)triethoxysilane

2,3,5,6-tetramethoxy-ω-(p-methoxybenzoyloxy)acetophenone

2,3,4,6-tetramethoxy-ο-(p-methoxybenzoyloxy)acetophenone

4-Methoxy-benzoate1-(3,5,5-trimethyl-cyclohex-2-enylidene)-pyrrolidinium;

Refernces

• 1、 Rouhi-Saadabad, Hamed,Akhlaghinia, Batool. "Facile and direct synthesis of symmetrical acid anhydrides using a newly prepared powerful and efficient mixed reagent". . p. 479 - 485. Retrieved 2015/01/30.
• 2、 Bhattacharya, Apurba,Patel, Nitin C.,Vasques, Tomas,Tichkule, Ritesh,Parmar, Gaurang,Wu, Jiejun. "Surfactant-mediated solvent-free dealkylative cleavage of ethers and esters and trans-alkylation under neutral conditions". . p. 565 - 567. Retrieved 2007/10/03.