2-broMo-1-(4-broMo-3-Methylphenyl)ethanone

Base Information

• Chemical Name: 2-broMo-1-(4-broMo-3-Methylphenyl)ethanone
• CAS No.: 3114-08-7
• Molecular Formula: C9H8Br2O
• Molecular Weight: 291.97
• Hs Code.: 2914700090
• Mol file: 3114-08-7.mol

Synonyms:2-broMo-1-(4-broMo-3-Methylphenyl)ethanone;4-Bromo-3-methylphenacylbromide,tech

Chemical Property of 2-broMo-1-(4-broMo-3-Methylphenyl)ethanone

Chemical Property:

• PSA: 17.07000
• LogP: 3.33510

Purity/Quality:

99%min. ^*data from raw suppliers

2-Bromo-1-(4-bromo-3-methylphenyl)ethanone tech% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-broMo-1-(4-broMo-3-Methylphenyl)ethanone

There total 8 articles about 2-broMo-1-(4-broMo-3-Methylphenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Trimethyl phenylammonium tribromide + 1-(4-bromo-3-methylphenyl)ethan-1-one (37074-40-1) → 2-bromo-1-(4-bromo-3-methylphenyl)ethan-1-one (3114-08-7)

Guidance literature:

In tetrahydrofuran;

Reference yield: 60.0%

1-(4-bromo-3-methylphenyl)ethan-1-one (37074-40-1) → 2-bromo-1-(4-bromo-3-methylphenyl)ethan-1-one (3114-08-7)

Guidance literature:

With copper(ll) bromide; In ethyl acetate; at 80 ℃; Inert atmosphere;

Reference yield:

tributyl(1-ethoxyvinyl)stannane (97674-02-7) + 1-bromo-4-iodo-2-methylbenzene (202865-85-8) → 2-bromo-1-(4-bromo-3-methylphenyl)ethan-1-one (3114-08-7)

Guidance literature:

tributyl(1-ethoxyvinyl)stannane; 1-bromo-4-iodo-2-methylbenzene; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; at 80 ℃; for 0.166667h; Inert atmosphere;

With N-Bromosuccinimide; In 1,4-dioxane; water; at 0 ℃; for 0.5h;

upstream raw materials:

tributyl(1-ethoxyvinyl)stannane

1-bromo-4-iodo-2-methylbenzene

1-(4-bromo-3-methylphenyl)ethan-1-one

1,4-dioxane

Downstream raw materials:

C₁₉H₂₄BrNO₅

Br^(1-)*C₂₇H₂₃BrOP⁽¹⁺⁾

1-(4-bromo-3-methylphenyl)-3-(3,5-dichlorophenyl)-4,4,4-trifluorobut-2-en-1-one

4-[3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-but-2-enoyl]-2-methyl-benzoic acid ethyl ester