3-iodo-1-[(4-methylphenyl)sulfonyl]-5-[5-(methylsulfinyl)-1,3,4-thiadiazol-2-yl]-1H-Indole

Base Information

Chemical Name:3-iodo-1-[(4-methylphenyl)sulfonyl]-5-[5-(methylsulfinyl)-1,3,4-thiadiazol-2-yl]-1H-Indole
CAS No.:1401350-38-6
Molecular Formula:C₁₈H₁₄IN₃O₃S₃
Molecular Weight:0
Hs Code.:
Mol file:1401350-38-6.mol

Synonyms:3-iodo-1-[(4-methylphenyl)sulfonyl]-5-[5-(methylsulfinyl)-1,3,4-thiadiazol-2-yl]-1H-Indole

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Chemical Property of 3-iodo-1-[(4-methylphenyl)sulfonyl]-5-[5-(methylsulfinyl)-1,3,4-thiadiazol-2-yl]-1H-Indole

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Technology Process of 3-iodo-1-[(4-methylphenyl)sulfonyl]-5-[5-(methylsulfinyl)-1,3,4-thiadiazol-2-yl]-1H-Indole

There total 3 articles about 3-iodo-1-[(4-methylphenyl)sulfonyl]-5-[5-(methylsulfinyl)-1,3,4-thiadiazol-2-yl]-1H-Indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1401348-65-9
2-(3-iodo-1-tosyl-1H-indol-5-yl)-5-(methylthio)-1,3,4-thiadiazole

: 1401350-38-6
2-(3-iodo-1-tosyl-1H-indol-5-yl)-5-(methylsulfinyl)-1,3,4-thiadiazole

: 1401348-66-0
2-(3-iodo-1-tosyl-1H-indol-5-yl)-5-(methylsulfonyl)-1,3,4-thiadiazole

Guidance literature:: With sodium tungstate; dihydrogen peroxide; In water; acetic acid; at 20 ℃; for 72h;

Reference yield:

: 1401348-60-4
2-(1H-indol-5-yl)-5-(methylthio)-1,3,4-thiadiazole

: 1401350-38-6
2-(3-iodo-1-tosyl-1H-indol-5-yl)-5-(methylsulfinyl)-1,3,4-thiadiazole

: 1401348-66-0
2-(3-iodo-1-tosyl-1H-indol-5-yl)-5-(methylsulfonyl)-1,3,4-thiadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide; iodine / N,N-dimethyl-formamide / 2 h / 20 °C

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 8 h / 20 °C

3: sodium tungstate; dihydrogen peroxide / water; acetic acid / 72 h / 20 °C

With sodium tungstate; dihydrogen peroxide; iodine; sodium hydride; potassium hydroxide; In water; acetic acid; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1401348-61-5
2-(3-iodo-1H-indol-5-yl)-5-(methylthio)-1,3,4-thiadiazole

: 1401350-38-6
2-(3-iodo-1-tosyl-1H-indol-5-yl)-5-(methylsulfinyl)-1,3,4-thiadiazole

: 1401348-66-0
2-(3-iodo-1-tosyl-1H-indol-5-yl)-5-(methylsulfonyl)-1,3,4-thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 8 h / 20 °C

2: sodium tungstate; dihydrogen peroxide / water; acetic acid / 72 h / 20 °C

With sodium tungstate; dihydrogen peroxide; sodium hydride; In water; acetic acid; N,N-dimethyl-formamide; mineral oil;