[1,2,4]Triazolo[1,5-a]pyridine-6-MethanaMine

Base Information

• Chemical Name: [1,2,4]Triazolo[1,5-a]pyridine-6-MethanaMine
• CAS No.: 943894-99-3
• Molecular Formula: C₇H₈N₄
• Molecular Weight: 148.167
• Hs Code.: 2933990090
• Mol file: 943894-99-3.mol

Synonyms:[1,2,4]Triazolo[1,5-a]pyridine-6-MethanaMine;[1,2,4]Triazolo[1,5-a]pyridin-6-ylMethanaMine

Chemical Property of [1,2,4]Triazolo[1,5-a]pyridine-6-MethanaMine

Chemical Property:

• PSA: 56.21000
• LogP: 0.88830

Purity/Quality:

97% ^*data from raw suppliers

[1,2,4]Triazolo[1,5-a]pyridin-6-ylmethanamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [1,2,4]Triazolo[1,5-a]pyridine-6-MethanaMine

There total 4 articles about [1,2,4]Triazolo[1,5-a]pyridine-6-MethanaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[1,2,4]triazolo[1,5-a]pyridine-6-carbonitrile (943845-23-6) → [1,2,4]triazolo[1,5-a]pyridin-6-ylmethanamine (943894-99-3)

Guidance literature:

With ammonia; hydrogen; In ethanol; at 20 ℃; for 2h;

DOI:10.1021/jm500510f

Reference yield:

6-aminonicotinonitrile (4214-73-7) → [1,2,4]triazolo[1,5-a]pyridin-6-ylmethanamine (943894-99-3)

Guidance literature:

Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 130 °C

2: pyridine; hydroxylamine-O-sulfonic acid / methanol / 20 °C

3: hydrogen; ammonia / ethanol / 2 h / 20 °C

With pyridine; ammonia; hydrogen; hydroxylamine-O-sulfonic acid; In methanol; ethanol; N,N-dimethyl-formamide;

DOI:10.1021/jm500510f

Reference yield:

N'-(5-cyanopyridin-2-yl)-N,N-dimethylformamidine (154924-17-1) → [1,2,4]triazolo[1,5-a]pyridin-6-ylmethanamine (943894-99-3)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; hydroxylamine-O-sulfonic acid / methanol / 20 °C

2: hydrogen; ammonia / ethanol / 2 h / 20 °C

With pyridine; ammonia; hydrogen; hydroxylamine-O-sulfonic acid; In methanol; ethanol;

DOI:10.1021/jm500510f

upstream raw materials:

6-aminonicotinonitrile

N'-(5-cyanopyridin-2-yl)-N,N-dimethylformamidine

[1,2,4]triazolo[1,5-a]pyridine-6-carbonitrile

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