methyl-13C ether

Base Information

• Chemical Name: methyl-13C ether
• CAS No.: 149228-22-8
• Molecular Formula: C2H6O
• Molecular Weight: 48.09
• Mol file: 149228-22-8.mol

Synonyms:DIMETHYL-13C2 ETHER;Dimethyl ether-13C2

Chemical Property of methyl-13C ether

Chemical Property:

• PSA: 9.23000
• LogP: 0.26260

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Hazard Codes: F+
• Statements: 12
• Safety Statements: 9-16-33

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl-13C ether

There total 1 articles about methyl-13C ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methane (6532-48-5) → [13C]methanol (14742-26-8) + 13C2-dimethyl ether (149228-22-8)

Guidance literature:

methane; at 200 ℃; for 0.5h; under 4500.45 Torr; Inert atmosphere; Schlenk technique;

With water; at 120 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

DOI:10.1002/anie.202105307

Reference yield:

4-methylethylbenzene (622-96-8) + 13C2-dimethyl ether (149228-22-8) → propene + [13C2]ethene (51915-19-6) + 13C-1,2,4,5-tetramethylbenzene (439669-20-2) + 13C9-4-ethyltoluene + 13C-1,2,4-trimethylbenzene (439669-09-7) + 13C2-p-xylene (116598-94-8)

Guidance literature:

With H-ZSM-5 zeolite catalyst; quartz sand; at 449.84 ℃; under 30.003 - 69.757 Torr; Temperature; Inert atmosphere;

DOI:10.1016/j.jcat.2013.11.003

upstream raw materials:

methane

Downstream raw materials:

[13C₂]ethene

¹³C-1,2,4,5-tetramethylbenzene

¹³C-1,2,4-trimethylbenzene

¹³C₂-p-xylene

Refernces