Methyl ether-13C2

Base Information

• Chemical Name: Methyl ether-13C2
• CAS No.: 149228-22-8
• Molecular Formula: C2H6O
• Molecular Weight: 48.09
• European Community (EC) Number: 694-311-4
• DSSTox Substance ID: DTXSID30482794
• Wikidata: Q82319507
• Mol file: 149228-22-8.mol

Synonyms:Methyl ether-13C2;149228-22-8;(113C)methoxy(113C)methane;DTXSID30482794;Dimethyl ether-13C2, 99 atom % 13C

Chemical Property of Methyl ether-13C2

Chemical Property:

• PSA: 9.23000
• LogP: 0.26260
• XLogP3: 0.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 48.048574481
• Heavy Atom Count: 3
• Complexity: 2.8

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Hazard Codes: F+
• Statements: 12
• Safety Statements: 9-16-33

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC
• Isomeric SMILES: [13CH3]O[13CH3]

Technology Process of Methyl ether-13C2

There total 1 articles about Methyl ether-13C2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methane (6532-48-5) → [13C]methanol (14742-26-8) + 13C2-dimethyl ether (149228-22-8)

Guidance literature:

methane; at 200 ℃; for 0.5h; under 4500.45 Torr; Inert atmosphere; Schlenk technique;

With water; at 120 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

DOI:10.1002/anie.202105307

Reference yield:

4-methylethylbenzene (622-96-8) + 13C2-dimethyl ether (149228-22-8) → propene + [13C2]ethene (51915-19-6) + 13C-1,2,4,5-tetramethylbenzene (439669-20-2) + 13C9-4-ethyltoluene + 13C-1,2,4-trimethylbenzene (439669-09-7) + 13C2-p-xylene (116598-94-8)

Guidance literature:

With H-ZSM-5 zeolite catalyst; quartz sand; at 449.84 ℃; under 30.003 - 69.757 Torr; Temperature; Inert atmosphere;

DOI:10.1016/j.jcat.2013.11.003

upstream raw materials:

methane

Downstream raw materials:

[13C₂]ethene

¹³C-1,2,4,5-tetramethylbenzene

¹³C-1,2,4-trimethylbenzene

¹³C₂-p-xylene