3-PYRIDINECARBOXYLIC ACID, 2,5-DICHLORO-, ETHYL ESTER

Base Information

• Chemical Name: 3-PYRIDINECARBOXYLIC ACID, 2,5-DICHLORO-, ETHYL ESTER
• CAS No.: 148065-10-5
• Molecular Formula: C8H7Cl2NO2
• Molecular Weight: 220.055
• Hs Code.: 2933399090
• Mol file: 148065-10-5.mol

Synonyms:3-PYRIDINECARBOXYLIC ACID, 2,5-DICHLORO-, ETHYL ESTER;ethyl 5-chloro-2-chloronicotinate

Chemical Property of 3-PYRIDINECARBOXYLIC ACID, 2,5-DICHLORO-, ETHYL ESTER

Chemical Property:

• PSA: 39.19000
• LogP: 2.56510

Purity/Quality:

98%min ^*data from raw suppliers

Ethyl 2,5-dichloronicotinate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-PYRIDINECARBOXYLIC ACID, 2,5-DICHLORO-, ETHYL ESTER

There total 5 articles about 3-PYRIDINECARBOXYLIC ACID, 2,5-DICHLORO-, ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethanol (64-17-5) + 2,5-dichloronicotinic acid (59782-85-3) → ethyl 5-chloro-2-chloronicotinate (148065-10-5)

Guidance literature:

With sulfuric acid; at 130 ℃; for 72h;

Reference yield: 99.0%

2,5-dichloronicotinic acid (59782-85-3) → ethyl 5-chloro-2-chloronicotinate (148065-10-5)

Guidance literature:

In toluene; at 100 ℃;

DOI:10.1021/acs.jmedchem.0c02274

Reference yield: 82.0%

C10H13ClN2O2 → ethyl 5-chloro-2-chloronicotinate (148065-10-5)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 40 ℃; for 5h;

DOI:10.1002/jlcr.1887

upstream raw materials:

ethyl 2,2-dichlorocyanoacetate

acrolein

ethanol

2,5-dichloronicotinic acid

Downstream raw materials:

ethyl 5-chloro-2-methylnicotinate

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