trans,trans-4-But-3-enyl-4''-pentyl-bicyclohexyl

Base Information

Chemical Name:trans,trans-4-But-3-enyl-4''-pentyl-bicyclohexyl
CAS No.:203864-69-1
Molecular Formula:C21H38
Molecular Weight:290.53
Hs Code.:
DSSTox Substance ID:DTXSID30705298
Nikkaji Number:J1.016.995J,J1.328.497K
Mol file:203864-69-1.mol

Synonyms:203864-69-1;TRANS,TRANS-4-BUT-3-ENYL-4''-PENTYL-BICYCLOHEXYL;DTXSID30705298;4-(3-Butenyl)-4'alpha-pentyl-1alpha,1'-bi[cyclohexane];4-(BUT-3-EN-1-YL)-4'-PENTYL-1,1'-BI(CYCLOHEXANE);4beta-(4beta-Pentylcyclohexane-1alpha-yl)-1alpha-(3-butenyl)cyclohexane

Suppliers and Price of trans,trans-4-But-3-enyl-4''-pentyl-bicyclohexyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of trans,trans-4-But-3-enyl-4''-pentyl-bicyclohexyl

Chemical Property:

PSA：0.00000
LogP:7.14570
XLogP3:9.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:8
Exact Mass:290.297351212
Heavy Atom Count:21
Complexity:264

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCC1CCC(CC1)C2CCC(CC2)CCC=C

Technology Process of trans,trans-4-But-3-enyl-4''-pentyl-bicyclohexyl

There total 2 articles about trans,trans-4-But-3-enyl-4''-pentyl-bicyclohexyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1826-67-1
vinyl magnesium bromide

: 291300-72-6
1-[trans-4-(2-iodoethyl)cyclohexyl]-trans-4-pentylcyclohexane

: 203864-69-1
1-[trans-4-(3-butenyl)cyclohexyl]-trans-4-pentylcyclohexane

Guidance literature:: With copper(l) iodide; In tetrahydrofuran; at -30 - 0 ℃;
DOI:10.1246/bcsj.73.1633

Reference yield:

: 129738-34-7
1-[trans-4-(ethenyl)cyclohexyl]-trans-4-pentylcyclohexane

: 203864-69-1
1-[trans-4-(3-butenyl)cyclohexyl]-trans-4-pentylcyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: borane; 2-methyl-2-butene / tetrahydrofuran / 11 h / 20 °C

1.2: 75 percent / iodine; methanol / tetrahydrofuran

2.1: 90 percent / copper(I) iodide / tetrahydrofuran / -30 - 0 °C

With copper(l) iodide; 2-methyl-but-2-ene; borane; In tetrahydrofuran; 1.1: hydroboration / 1.2: Iodination / 2.1: Alkylation;
DOI:10.1246/bcsj.73.1633