(4-OXO-6-PHENYL-1,4-DIHYDRO-PYRIMIDIN-2-YL-SULFANYL)-ACETIC ACID

Base Information

• Chemical Name: (4-OXO-6-PHENYL-1,4-DIHYDRO-PYRIMIDIN-2-YL-SULFANYL)-ACETIC ACID
• CAS No.: 67466-26-6
• Molecular Formula: C12H10N2O3S
• Molecular Weight: 262.28
• Hs Code.: 2933599090

Synonyms:(4-OXO-6-PHENYL-1,4-DIHYDRO-PYRIMIDIN-2-YL-SULFANYL)-ACETIC ACID;[(4-OXO-6-PHENYL-1,4-DIHYDROPYRIMIDIN-2-YL)THIO]ACETIC ACID;[(4-Oxo-6-phenyl-1,4-dihydro-2-pyrimidinyl)sulfanyl]acetic acid

Chemical Property of (4-OXO-6-PHENYL-1,4-DIHYDRO-PYRIMIDIN-2-YL-SULFANYL)-ACETIC ACID

Chemical Property:

• PSA: 108.35000
• LogP: 1.61360

Purity/Quality:

98%min ^*data from raw suppliers

(4-Hydroxy-6-phenyl-pyrimidin-2-ylsulfanyl)-aceticacid 95%+ ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (4-OXO-6-PHENYL-1,4-DIHYDRO-PYRIMIDIN-2-YL-SULFANYL)-ACETIC ACID

There total 2 articles about (4-OXO-6-PHENYL-1,4-DIHYDRO-PYRIMIDIN-2-YL-SULFANYL)-ACETIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

6-phenyl-2-thiouracil (36822-11-4) + chloroacetic acid (79-11-8) → 6-Phenyl-2-S-carboxymethylpyrimidine-4-one (67466-26-6)

Guidance literature:

With sodium ethanolate; In ethanol; Heating;

DOI:10.1515/znb-1999-0614

Reference yield:

ethyl 3-oxo-3-phenylpropionate (94-02-0) → 6-Phenyl-2-S-carboxymethylpyrimidine-4-one (67466-26-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / sodium acetate / ethanol

2: 66 percent / EtONa / ethanol / Heating

With sodium ethanolate; sodium acetate; In ethanol; 1: Cyclization / 2: Substitution;

DOI:10.1515/znb-1999-0614

upstream raw materials:

6-phenyl-2-thiouracil

chloroacetic acid

ethyl 3-oxo-3-phenylpropionate

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