N-(2-Amino-4-bromophenyl)-2-chloropropanamide

Base Information

Chemical Name:N-(2-Amino-4-bromophenyl)-2-chloropropanamide
CAS No.:868771-37-3
Molecular Formula:C9H10BrClN2O
Molecular Weight:277.5455
Hs Code.:2924299090
DSSTox Substance ID:DTXSID30468331
Mol file:868771-37-3.mol

Synonyms:N-(2-Amino-4-bromophenyl)-2-chloropropanamide;868771-37-3;DTXSID30468331

Suppliers and Price of N-(2-Amino-4-bromophenyl)-2-chloropropanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
N-(2-Amino-4-bromophenyl)-2-chloropropanamide 95+%
1g
$ 377.00

American Custom Chemicals Corporation
N-(2-AMINO-4-BROMOPHENYL)-2-CHLOROPROPANAMIDE 95.00%
5MG
$ 504.88

Total 3 raw suppliers

Chemical Property of N-(2-Amino-4-bromophenyl)-2-chloropropanamide

Chemical Property:

PSA：58.61000
LogP:3.82780
Storage Temp.:2-8°C
XLogP3:2.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:275.96650
Heavy Atom Count:14
Complexity:215

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

N-(2-Amino-4-bromophenyl)-2-chloropropanamide 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C(=O)NC1=C(C=C(C=C1)Br)N)Cl

Technology Process of N-(2-Amino-4-bromophenyl)-2-chloropropanamide

There total 4 articles about N-(2-Amino-4-bromophenyl)-2-chloropropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 868771-26-0
N-(4-bromo-2-nitro-phenyl)-2-chloro-propionamide

: 868771-37-3
N-(2-amino-4-bromo-phenyl)-2-chloro-propionamide

Guidance literature:: With iron; ammonium chloride; acetic acid; In water; N,N-dimethyl-formamide; at 50 ℃; for 0.25h;
DOI:10.3987/COM-05-10461

Reference yield:

: 21262-08-8
N-(4-bromophenyl)-2-chloropropanamide

: 868771-37-3
N-(2-amino-4-bromo-phenyl)-2-chloro-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / KNO₃ / H₂SO₄ / 1 h / 20 °C

2: 93 percent / Fe; NH₄Cl; AcOH / H₂O; dimethylformamide / 0.25 h / 50 °C

With iron; ammonium chloride; acetic acid; potassium nitrate; In sulfuric acid; water; N,N-dimethyl-formamide;
DOI:10.3987/COM-05-10461

Reference yield:

: 106-40-1
4-bromo-aniline

: 868771-37-3
N-(2-amino-4-bromo-phenyl)-2-chloro-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / toluene / 1 h / 120 °C

2: 94 percent / KNO₃ / H₂SO₄ / 1 h / 20 °C

3: 93 percent / Fe; NH₄Cl; AcOH / H₂O; dimethylformamide / 0.25 h / 50 °C

With iron; ammonium chloride; acetic acid; potassium nitrate; In sulfuric acid; water; N,N-dimethyl-formamide; toluene;
DOI:10.3987/COM-05-10461