2-Pyridinecarboxylic acid, 4-broMo-6-Methyl-, ethyl ester

Base Information

Chemical Name:2-Pyridinecarboxylic acid, 4-broMo-6-Methyl-, ethyl ester
CAS No.:947179-03-5
Molecular Formula:C₉H₁₀BrNO₂
Molecular Weight:244.088
Hs Code.:
Mol file:947179-03-5.mol

Synonyms:2-Pyridinecarboxylic acid, 4-broMo-6-Methyl-, ethyl ester

Suppliers and Price of 2-Pyridinecarboxylic acid, 4-broMo-6-Methyl-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
Ethyl4-bromo-6-methylpicolinate
1g
$ 3039.75

Alichem
Ethyl4-bromo-6-methylpicolinate
250mg
$ 1029.00

Total 4 raw suppliers

Chemical Property of 2-Pyridinecarboxylic acid, 4-broMo-6-Methyl-, ethyl ester

Chemical Property:

PSA：39.19000
LogP:2.32920
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

98% ^*data from raw suppliers

Ethyl4-bromo-6-methylpicolinate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Pyridinecarboxylic acid, 4-broMo-6-Methyl-, ethyl ester

There total 5 articles about 2-Pyridinecarboxylic acid, 4-broMo-6-Methyl-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 64-17-5
ethanol

: 1122090-59-8
potassium 4-bromo-6-methylpyridine-2-carboxylic acid

: 947179-03-5
ethyl 4-bromo-6-methylpicolinate

Guidance literature:: With sulfuric acid; at 70 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jm4014696

Reference yield:

: 64-17-5
ethanol

: 30235-16-6
6-methyl-4-nitropyridine-2-carboxylic acid

: 947179-03-5
ethyl 4-bromo-6-methylpicolinate

Guidance literature:: ethanol; 6-methyl-4-nitropyridine-2-carboxylic acid; With sulfuric acid; for 8h; Heating / reflux;

With sodium carbonate; In water; pH=7;

Reference yield:

: 22282-99-1
4-bromo-2-methylpyridine

: 947179-03-5
ethyl 4-bromo-6-methylpicolinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / Reflux

1.2: 3 h / Reflux

2.1: potassium permanganate / acetone / 2 h / 40 °C

3.1: sulfuric acid / 16 h / 70 °C

With potassium permanganate; sulfuric acid; In acetone;