N~1~-benzyl-2-methylpropane-1,2-diamine

Base Information

Chemical Name:N~1~-benzyl-2-methylpropane-1,2-diamine
CAS No.:80704-02-5
Molecular Formula:C11H18N2
Molecular Weight:178.277
Hs Code.:

Synonyms:1,2-PropanediaMine, 2-Methyl-N1-(phenylMethyl)-

Suppliers and Price of N~1~-benzyl-2-methylpropane-1,2-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of N~1~-benzyl-2-methylpropane-1,2-diamine

Chemical Property:

Vapor Pressure:0.00381mmHg at 25°C
Boiling Point:280.3°C at 760 mmHg
Flash Point:143°C
Density:0.967g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N~1~-benzyl-2-methylpropane-1,2-diamine

There total 3 articles about N~1~-benzyl-2-methylpropane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 741221-17-0
N-benzyl-2-methyl-2-nitropropan-1-amine

: 80704-02-5
N¹-benzyl-2-methylpropane-1,2-diamine

Guidance literature:: With acetic acid; zinc; In tetrahydrofuran; at 0 - 20 ℃; for 29h; Inert atmosphere;
DOI:10.1039/c7ob02486j

Reference yield: 52.0%

: 100-52-7
benzaldehyde

: 811-93-8
1,1-dimethylethylenediamine

: 80704-02-5
N¹-benzyl-2-methylpropane-1,2-diamine

Guidance literature:: benzaldehyde; 1,1-dimethylethylenediamine; With magnesium sulfate; In methanol; at 20 ℃; for 0.5h; Inert atmosphere;

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jacs.6b12234

Reference yield:

: 100-46-9
benzylamine

: 80704-02-5
N¹-benzyl-2-methylpropane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

2: Raney nickel; methanol / 30 - 50 °C / 25742.8 Torr / Hydrogenation

With methanol; nickel;