Benzamide, N-(2-methoxyphenyl)-2-methyl-

Base Information

• Chemical Name: Benzamide, N-(2-methoxyphenyl)-2-methyl-
• CAS No.: 55814-34-1
• Molecular Formula: C15H15NO2
• Molecular Weight: 241.2851
• European Community (EC) Number: 666-795-7
• NSC Number: 29489
• DSSTox Substance ID: DTXSID40204404
• Nikkaji Number: J3.098.587G
• Wikidata: Q83077838
• ChEMBL ID: CHEMBL1214634

Synonyms:N-(2-methoxyphenyl)-2-methylbenzamide;Benzamide, N-(2-methoxyphenyl)-2-methyl-;55814-34-1;NSC29489;AI3-31269;Oprea1_874784;CHEMBL1214634;SCHEMBL11784909;DTXSID40204404;NSC 29489;NSC-29489;STK086120;AKOS000491190;CS-0362117;Z27797508

Chemical Property of Benzamide, N-(2-methoxyphenyl)-2-methyl-

Chemical Property:

• Vapor Pressure: 0.000469mmHg at 25°C
• Boiling Point: 314.3°Cat760mmHg
• Flash Point: 143.9°C
• Density: 1.156g/cm³
• XLogP3: 2.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 241.110278721
• Heavy Atom Count: 18
• Complexity: 280

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=CC=C1C(=O)NC2=CC=CC=C2OC

Technology Process of Benzamide, N-(2-methoxyphenyl)-2-methyl-

There total 3 articles about Benzamide, N-(2-methoxyphenyl)-2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-methoxy-phenylamine (90-04-0) + ortho-toluoyl chloride (933-88-0) → N-(2-methoxyphenyl)-2-methylbenzamide (55814-34-1)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;

DOI:10.1016/j.bmc.2010.06.034

Reference yield:

N-methyl-2-phenyl-benzoxazolium iodide (61372-51-8) + furan-2,3,5(4H)-trione pyridine (1:1) + dimethyl sulfate (77-78-1) → N-(2-methoxyphenyl)-2-methylbenzamide (55814-34-1)

Guidance literature:

Reference yield:

→ N-(2-methoxyphenyl)-2-methylbenzamide (55814-34-1)

Guidance literature:

2-Methylbenzoesaeureester, o-Anisidin;

upstream raw materials:

N-methyl-2-phenyl-benzoxazolium iodide

dimethyl sulfate

2-methoxy-phenylamine

ortho-toluoyl chloride

Downstream raw materials:

N-(2'-methoxyphenyl)-1-isoindolinone

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