Technology Process of Samarium phosphide
There total 2 articles about Samarium phosphide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
neat (no solvent);
heating Sm and red P in a sealed quartz ampoule at 1100°C for 20 h under pressure of 6.6E-3 Pa, rate of raising temp. from 300 to 1100°C less than 1°C/min., regrinding, pelleting, sintering at 1100°C for 10 h and 6.6E-3 Pa;
- Guidance literature:
-
In
neat (no solvent);
heating (sealed Vycor glass tube, vac. 1E-6 Torr, 1°C/min to 500°C, 16 h at this temp., then 750°C, 15 days);
DOI:10.1103/PhysRevB.20.1985
