2,6-DICHLOROACETOACETANILID

Base Information

• Chemical Name: 2,6-DICHLOROACETOACETANILID
• CAS No.: 414906-63-1
• Molecular Formula: C₁₀H₉Cl₂NO₂
• Molecular Weight: 246.093
• Mol file: 414906-63-1.mol

Synonyms:2,6-DICHLOROACETOACETANILID;2,6-DICHLOROACETOACETANILIDE;N-(2,6-DICHLOROPHENYL)-3-OXOBUTANAMIDE

Chemical Property of 2,6-DICHLOROACETOACETANILID

Chemical Property:

• Boiling Point: 407.9±45.0 °C(Predicted)
• PKA: 10.52±0.46(Predicted)
• PSA: 46.17000
• Density: 1.393±0.06 g/cm3(Predicted)
• LogP: 2.98400

Purity/Quality:

97% ^*data from raw suppliers

N-(2,6-DICHLOROPHENYL)-3-OXOBUTANAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-DICHLOROACETOACETANILID

There total 1 articles about 2,6-DICHLOROACETOACETANILID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyleneoxetan-2-one (674-82-8,2130-41-8) + 2,6-Dichloroaniline (608-31-1) → C10H9Cl2NO2 (414906-63-1)

Guidance literature:

In benzene; Heating;

DOI:10.1016/j.tetlet.2008.05.132

Reference yield:

C10H9Cl2NO2 (414906-63-1) → 2-Chloro-N-(2,6-dichloro-phenyl)-3-oxo-butyramide (1053235-94-1)

Guidance literature:

With thionyl chloride; In benzene; at 20 ℃;

DOI:10.1016/j.tetlet.2008.05.132

upstream raw materials:

4-methyleneoxetan-2-one

2,6-Dichloroaniline

Downstream raw materials:

2-Chloro-N-(2,6-dichloro-phenyl)-3-oxo-butyramide

Refernces