3β-Methoxymethoxycholest-5-ene

Base Information

• Chemical Name: 3β-Methoxymethoxycholest-5-ene
• CAS No.: 2626-17-7
• Molecular Formula: C29H50O2
• Molecular Weight: 430.71
• Mol file: 2626-17-7.mol

Synonyms:3β-(Methoxymethoxy)cholest-5-ene;3β-Methoxymethoxycholest-5-ene;Formaldehyde methyl 3β-cholesteryl acetal

Chemical Property of 3β-Methoxymethoxycholest-5-ene

Chemical Property:

• PSA: 18.46000
• LogP: 8.01690

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3β-Methoxymethoxycholest-5-ene

There total 6 articles about 3β-Methoxymethoxycholest-5-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

Dimethoxymethane (109-87-5) + cholesterol (57-88-5) → 3β-methoxymethoxy-5-cholestene (2626-17-7)

Guidance literature:

With Envirocat EPZG^R; In dichloromethane; at 40 ℃; for 3.5h;

Reference yield: 76.0%

Dimethoxymethane (109-87-5) + cholesterol (765935-41-9) → Cholesterol-MOM (2626-17-7)

Guidance literature:

iodine; allyl-trimethyl-silane; In benzene; for 5h; Ambient temperature;

DOI:10.1055/s-1983-30554

Reference yield: 69.0%

methoxymethyl acetate (4382-76-7) + cholesterol (57-88-5) → 3β-methoxymethoxy-5-cholestene (2626-17-7)

Guidance literature:

With zinc(II) chloride; In diethyl ether; dichloromethane; for 16h; Ambient temperature;

upstream raw materials:

Dimethoxymethane

cholesterol

cholesterol

methoxymethyl acetate

Downstream raw materials:

(3S,8S,9S,10R,13R,14S,17R)-10,13-dimethyl-17-((R)-6-methylheptan-2-yl)-3-((3-phenylprop-2-yn-1-yl)oxy)-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthrene

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