trans-3-[[(1,1-DiMethylethyl)diMethylsilyl]oxy]cyclobutanol

Base Information

• Chemical Name: trans-3-[[(1,1-DiMethylethyl)diMethylsilyl]oxy]cyclobutanol
• CAS No.: 1408075-44-4
• Molecular Formula: C₁₀H₂₂O₂Si
• Molecular Weight: 202.369
• Hs Code.: 2906190090
• Mol file: 1408075-44-4.mol

Synonyms:trans-3-[[(1,1-DiMethylethyl)diMethylsilyl]oxy]cyclobutanol;trans-3-((tert-Butyldimethylsilyl)oxy)cyclobutanol

Chemical Property of trans-3-[[(1,1-DiMethylethyl)diMethylsilyl]oxy]cyclobutanol

Chemical Property:

• Boiling Point: 224.0±33.0 °C(Predicted)
• PKA: 14.76±0.40(Predicted)
• Density: 0.93±0.1 g/cm3(Predicted)
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

trans-3-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]cyclobutanol 97.0% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of trans-3-[[(1,1-DiMethylethyl)diMethylsilyl]oxy]cyclobutanol

There total 5 articles about trans-3-[[(1,1-DiMethylethyl)diMethylsilyl]oxy]cyclobutanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

(3-benzyloxycyclobutoxy)(tert-butyl)dimethylsilane → (1s,3s)-3-((tert-butyldimethylsilyl)oxy)cyclobutan-1-ol (1408074-89-4,1408075-44-4)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; at 25 ℃; for 3h; under 2585.81 Torr;

Reference yield:

3-(tert-butyldimethylsilyloxy)cyclobutyl pivalate (1089709-06-7) → 3-((tert-butyl dimethylsilyl)oxy)cyclobutan-1-ol (1089709-08-9,1408074-89-4,1408075-44-4)

Guidance literature:

With diisobutylaluminium hydride; In tetrahydrofuran; hexanes; at 0 ℃; for 1h;

Reference yield:

(3-benzyloxycyclobutoxy)-tert-butyl-dimethylsilane → 3-((tert-butyl dimethylsilyl)oxy)cyclobutan-1-ol (1089709-08-9,1408074-89-4,1408075-44-4)

Guidance literature:

With hydrogen; palladium(II) hydroxide; In methanol; at 60 ℃; for 16h; under 2585.81 Torr;

upstream raw materials:

3-(tert-butyldimethylsilyloxy)cyclobutyl pivalate

3-((tert-butyldimethylsilyl)oxy)cyclobutan-1-one

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