Cyclohexanecarboxylic acid, 1-(2-chloroethyl)-4-[[(1,1-diMethylethyl)diMethylsilyl]oxy]-, ethyl ester

Base Information

Chemical Name:Cyclohexanecarboxylic acid, 1-(2-chloroethyl)-4-[[(1,1-diMethylethyl)diMethylsilyl]oxy]-, ethyl ester
CAS No.:1097729-64-0
Molecular Formula:C17H33ClO3Si
Molecular Weight:348.986
Hs Code.:
Mol file:1097729-64-0.mol

Synonyms:Cyclohexanecarboxylic acid, 1-(2-chloroethyl)-4-[[(1,1-diMethylethyl)diMethylsilyl]oxy]-, ethyl ester

Suppliers and Price of Cyclohexanecarboxylic acid, 1-(2-chloroethyl)-4-[[(1,1-diMethylethyl)diMethylsilyl]oxy]-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Ethyl4-((tert-butyldimethylsilyl)oxy)-1-(2-chloroethyl)cyclohexanecarboxylate 95+%
1g
$ 772.00

Chemenu
ethyl4-((tert-butyldimethylsilyl)oxy)-1-(2-chloroethyl)cyclohexane-1-carboxylate 95%
1g
$ 729.00

American Custom Chemicals Corporation
ETHYL-4-((TERT-BUTYLDIMETHYLSILYL)OXY)-1-(2-CHLOROETHYL)CYCLOHEXANECARBOXYLATE 95.00%
5MG
$ 498.37

Total 7 raw suppliers

Chemical Property of Cyclohexanecarboxylic acid, 1-(2-chloroethyl)-4-[[(1,1-diMethylethyl)diMethylsilyl]oxy]-, ethyl ester

Chemical Property:

PSA：35.53000
LogP:5.12920
Storage Temp.:2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

Ethyl4-((tert-butyldimethylsilyl)oxy)-1-(2-chloroethyl)cyclohexanecarboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexanecarboxylic acid, 1-(2-chloroethyl)-4-[[(1,1-diMethylethyl)diMethylsilyl]oxy]-, ethyl ester

There total 2 articles about Cyclohexanecarboxylic acid, 1-(2-chloroethyl)-4-[[(1,1-diMethylethyl)diMethylsilyl]oxy]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1097729-64-0
ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-(2-chloroethyl)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

2.2: 3 h / -78 - 20 °C

With 1H-imidazole; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 3618-04-0,75877-66-6,17159-80-7
4-hydroxycyclohexyl carboxylic acid ethyl ester

: 1097729-64-0
ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-(2-chloroethyl)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

2.2: 3 h / -78 - 20 °C

With 1H-imidazole; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;