N-BOC-2-thia-6-azaspiro[3.3]heptane 2,2-dioxide

Base Information

• Chemical Name: N-BOC-2-thia-6-azaspiro[3.3]heptane 2,2-dioxide
• CAS No.: 1291487-31-4
• Molecular Formula: C₁₀H₁₇NO₄S
• Molecular Weight: 247.315
• Hs Code.: 2934999090
• Mol file: 1291487-31-4.mol

Synonyms:N-BOC-2-thia-6-azaspiro[3.3]heptane 2,2-dioxide;6-Boc-2-Thia-6-aza-spiro[3.3]heptane-2,2-dioxide;6-Boc-2-Thia-6-aza-spiro[...;2-Thia-6-azaspiro[3.3]heptane, 2,2-dioxide-6-carboxylic acid tert-butyl ester;tert-Butyl 2-thia-6-azaspiro[3.3]heptane-6-carboxylate 2,2-dioxide

Chemical Property of N-BOC-2-thia-6-azaspiro[3.3]heptane 2,2-dioxide

Chemical Property:

• PSA: 72.06000
• LogP: 1.67060

Purity/Quality:

99%, ^*data from raw suppliers

2-Thia-6-azaspiro[3.3]heptane,2,2-dioxide-6-carboxylicacidtert-butylester 97.0% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-BOC-2-thia-6-azaspiro[3.3]heptane 2,2-dioxide

There total 3 articles about N-BOC-2-thia-6-azaspiro[3.3]heptane 2,2-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

tert-butyl 2-thia-6-azaspiro[3.3]heptane-6-carboxylate → N-Boc-2-thia-6-azaspiro[3.3]heptane 2,2-dioxide (1291487-31-4)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 1.16667h;

Reference yield:

2-thia-6-azaspiro[3.3]heptane (920491-09-4) → N-Boc-2-thia-6-azaspiro[3.3]heptane 2,2-dioxide (1291487-31-4)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 20 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.17 h / 0 - 20 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → N-Boc-2-thia-6-azaspiro[3.3]heptane 2,2-dioxide (1291487-31-4)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 20 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.17 h / 0 - 20 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

upstream raw materials:

2-thia-6-azaspiro[3.3]heptane

di-tert-butyl dicarbonate

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