Anthranilic Acid-13C6

Base Information

• Chemical Name: Anthranilic Acid-13C6
• CAS No.: 335081-06-6
• Molecular Formula: C7H7NO2
• Molecular Weight: 143.072
• Mol file: 335081-06-6.mol

Synonyms:Anthranilic Acid-13C6;2-AA-13C6

Chemical Property of Anthranilic Acid-13C6

Chemical Property:

• PSA: 63.32000
• LogP: 1.54820

Purity/Quality:

99% ,98%,Electron Grade , ^*data from raw suppliers

Anthranilicacid-[13C6] ≥95% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Anthranilic Acid-13C6

There total 2 articles about Anthranilic Acid-13C6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C6(13)C6H15NO4 (176850-22-9) → 13C6-anthranilic acid (335081-06-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

DOI:10.1002/jlcr.1293

Reference yield:

N-Boc-aniline-[phenyl-13C6] (176850-21-8) → 13C6-anthranilic acid (335081-06-6)

Guidance literature:

Multi-step reaction with 2 steps

1: t-BuLi

2: TFA / CH₂Cl₂

With tert.-butyl lithium; trifluoroacetic acid; In dichloromethane;

DOI:10.1002/jlcr.1293

Reference yield: 80.0%

13C6-anthranilic acid (335081-06-6) + ethanol (64-17-5) → ethyl 2-amino[13C6]benzoate

Guidance literature:

With hydrogenchloride; at 60 ℃; for 1h;

DOI:10.1074/jbc.AC118.007225

upstream raw materials:

C₆⁽¹³⁾C₆H₁₅NO₄

N-Boc-aniline-[phenyl-13C₆]