(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)dimethylamine oxide

Base Information

• Chemical Name: (4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)dimethylamine oxide
• CAS No.: 30295-52-4
• Molecular Formula: C₁₃H₁₂F₁₇NO
• Molecular Weight: 521.217
• Mol file: 30295-52-4.mol

Synonyms:Undecylamine,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-N,N-dimethyl-, N-oxide(8CI)

Chemical Property of (4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)dimethylamine oxide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)dimethylamine oxide

There total 5 articles about (4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl)dimethylamine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

Dimethyl-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecyl)amine (148171-75-9) → N,N-dimethyl, N-<(3-F-octyl)propyl> amine oxide (30295-52-4)

Guidance literature:

With dihydrogen peroxide; In acetic acid; at 80 ℃; for 16h;

DOI:10.1016/0223-5234(92)90020-2

Reference yield:

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoic acid (34598-33-9) → N,N-dimethyl, N-<(3-F-octyl)propyl> amine oxide (30295-52-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 95 percent / SOCl₂ / Heating

2: 92 percent / diethyl ether / 2 h / Heating

3: 82 percent / LiAlH₄ / diethyl ether / 48 h / Ambient temperature

4: 45 percent / 30percent H₂O₂ / acetic acid / 16 h / 80 °C

With lithium aluminium tetrahydride; thionyl chloride; dihydrogen peroxide; In diethyl ether; acetic acid;

DOI:10.1016/0223-5234(92)90020-2

Reference yield:

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoylchloride (89373-67-1) → N,N-dimethyl, N-<(3-F-octyl)propyl> amine oxide (30295-52-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / diethyl ether / 2 h / Heating

2: 82 percent / LiAlH₄ / diethyl ether / 48 h / Ambient temperature

3: 45 percent / 30percent H₂O₂ / acetic acid / 16 h / 80 °C

With lithium aluminium tetrahydride; dihydrogen peroxide; In diethyl ether; acetic acid;

DOI:10.1016/0223-5234(92)90020-2

upstream raw materials:

Dimethyl-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-Heptadecafluoro-undecyl)amine

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoic acid

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecanoylchloride

N,N-dimethyl 3-(F-octyl)-propanamide