δ-Oxo-α-phenylbenzenepentanenitrile

Base Information

Chemical Name:δ-Oxo-α-phenylbenzenepentanenitrile
CAS No.:22228-41-7
Molecular Formula:C17H15NO
Molecular Weight:249.31
Hs Code.:
Mol file:22228-41-7.mol

Synonyms:δ-Oxo-α-phenylbenzenepentanenitrile

Suppliers and Price of δ-Oxo-α-phenylbenzenepentanenitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of δ-Oxo-α-phenylbenzenepentanenitrile

Chemical Property:

Melting Point:44 - 45 °C (petroleum ether)
PSA：40.86000
LogP:3.95688

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of δ-Oxo-α-phenylbenzenepentanenitrile

There total 8 articles about δ-Oxo-α-phenylbenzenepentanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 15295-43-9
1-benzoyl-2-phenylcyclopropane

: 7677-24-9
trimethylsilyl cyanide

: 22228-41-7
5-oxo-2,5-diphenylpentanenitrile

Guidance literature:: With tetrakis(acetonitrile)copper(I)tetrafluoroborate; 10-phenyl-10H-phenothiazine; lanthanum(lll) triflate; {3aS-[2(3'aR*,8'aS*),3aα,8aα]}-2,2'-(cyclopropylidene)-bis{3a,8a-dihydro-8H-indeno[1,2-d]-oxazole}; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Reagent/catalyst; Solvent; Schlenk technique; Sealed tube; Inert atmosphere; Irradiation; Green chemistry;
DOI:10.1039/d0cc05167e

Reference yield: 46.0%

: 140-29-4
phenylacetonitrile

: 768-03-6,26742-84-7
Phenyl vinyl ketone

: 22228-41-7
5-oxo-2,5-diphenylpentanenitrile

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 2,9-dihexyl-4,7-diphenyl-1,10-phenanthroline; sodium hydrogencarbonate; In toluene; at 80 ℃; for 24h; Time; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.1c02074

Reference yield: 33.0%

: benzene

: 22228-41-7
5-oxo-2,5-diphenylpentanenitrile

Guidance literature:: With dipotassium peroxodisulfate; [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; tetrabutyl-ammonium chloride; In water; for 17h; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.8b04104