3-(tert-butoxycarbonyl)-2,2-dimethyloxazolidine-4-carboxylic acid

Base Information

• Chemical Name: 3-(tert-butoxycarbonyl)-2,2-dimethyloxazolidine-4-carboxylic acid
• CAS No.: 301155-28-2
• Molecular Formula: C₁₁H₁₉NO₅
• Molecular Weight: 245.276
• Mol file: 301155-28-2.mol

Synonyms:3-(tert-butoxycarbonyl)-2,2-dimethyloxazolidine-4-carboxylic acid

Chemical Property of 3-(tert-butoxycarbonyl)-2,2-dimethyloxazolidine-4-carboxylic acid

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

3-(tert-Butoxycarbonyl)-2,2-dimethyl-1,3-oxazolidine-4-carboxylic acid 95%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 3-(tert-butoxycarbonyl)-2,2-dimethyloxazolidine-4-carboxylic acid

There total 14 articles about 3-(tert-butoxycarbonyl)-2,2-dimethyloxazolidine-4-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(S)-2,2-dimethyl-oxazolidine-3,4-dicarboxylic acid 3-tert-butyl ester 4-methyl ester (95715-86-9,108149-60-6) → (S)-3-(tert-butoxycarbonyl)-2,2-dimethyloxazolidine-4-carboxylic acid (139009-66-8,301155-28-2)

Guidance literature:

With lithium hydroxide monohydrate; water; In tetrahydrofuran; at 20 ℃; for 12h;

Reference yield: 99.0%

methyl [(4R)-3-(tert-butoxycarbonyl)-2,2-dimethyl-1,3-oxazolidin-4-yl]carboxylate (108149-60-6,95715-86-9) → (4R)-3-(tert-butoxycarbonyl)-2,2-dimethyl-1,3-oxazolidine-4-carboxylic acid (660852-86-8,301155-28-2)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; for 5.66667h;

DOI:10.1016/j.tetasy.2004.11.035

Reference yield: 88.0%

(R)-N-tert-butoxycarbonyl serine (3262-72-4,3850-40-6,6368-20-3,90582-28-8,84311-18-2) + 2,2-dimethoxy-propane (77-76-9) → (4R)-3-(tert-butoxycarbonyl)-2,2-dimethyl-1,3-oxazolidine-4-carboxylic acid (660852-86-8,301155-28-2)

Guidance literature:

With sulfuric acid; In acetone; at 0 - 30 ℃; for 0.5h;

upstream raw materials:

(S)-N-(tert-butoxycarbonyl)serine

2,2-dimethoxy-propane

(S)-2,2-dimethyl-oxazolidine-3,4-dicarboxylic acid 3-tert-butyl ester 4-methyl ester

di-tert-butyl dicarbonate

Downstream raw materials:

(S)-2,2-dimethyl-oxazolidine-3,4-dicarboxylic acid 3-tert-butyl ester 4-methyl ester

C₂₇H₂₈N₄O₆S₂

C₂₆H₂₆N₄O₆S₂

C₄₃H₅₀N₈O₁₀S₂

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