(E)-1-(4-hydroxy-3-methoxyphenyl)dec-1-en-3-one

Base Information

Chemical Name:(E)-1-(4-hydroxy-3-methoxyphenyl)dec-1-en-3-one
CAS No.:53172-10-4
Molecular Formula:C17H24 O3
Molecular Weight:276.376
Hs Code.:2914509090
Nikkaji Number:J1.554.378G,J3.189.709B
Wikidata:Q76386661
ChEMBL ID:CHEMBL4093796
Mol file:53172-10-4.mol

Synonyms:dehydroparadol

Suppliers and Price of (E)-1-(4-hydroxy-3-methoxyphenyl)dec-1-en-3-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of (E)-1-(4-hydroxy-3-methoxyphenyl)dec-1-en-3-one

Chemical Property:

Vapor Pressure:9.25E-08mmHg at 25°C
Boiling Point:423.2°Cat760mmHg
Flash Point:148.4°C
PSA：46.53000
Density:1.04g/cm³
LogP:4.34360
XLogP3:4.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:9
Exact Mass:276.17254462
Heavy Atom Count:20
Complexity:299

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCC(=O)C=CC1=CC(=C(C=C1)O)OC
Isomeric SMILES:CCCCCCCC(=O)/C=C/C1=CC(=C(C=C1)O)OC

Technology Process of (E)-1-(4-hydroxy-3-methoxyphenyl)dec-1-en-3-one

There total 6 articles about (E)-1-(4-hydroxy-3-methoxyphenyl)dec-1-en-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.3%

: 821-55-6
2-Nonanone

: 121-33-5,8014-42-4
vanillin

: 53172-10-4,878006-06-5
1-(4-hydroxy-3-methoxy-phenyl)-dec-1-en-3-one

Guidance literature:: In N,N-dimethyl-formamide; for 3h; Reflux;

Reference yield: 80.0%

: C₁₉H₂₆O₄

: 53172-10-4,878006-06-5
1-(4-hydroxy-3-methoxy-phenyl)-dec-1-en-3-one

Guidance literature:: With water; lithium hydroxide; In methanol; at 20 ℃; for 0.0833333h;

Reference yield:

: 821-55-6
2-Nonanone

: 53172-10-4,878006-06-5
1-(4-hydroxy-3-methoxy-phenyl)-dec-1-en-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.58 h / -78 °C

2: toluene-4-sulfonic acid / toluene / 0.08 h / Reflux

3: lithium hydroxide / tetrahydrofuran; methanol; water / 0.08 h / 20 °C

With n-butyllithium; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; water; toluene;
DOI:10.1016/j.freeradbiomed.2016.03.026