Technology Process of trans-3-Amino-1-methylcyclobutanol
There total 10 articles about trans-3-Amino-1-methylcyclobutanol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
methanol;
for 16h;
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethanol;
at 20 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: water; potassium hydroxide / ethanol / 16 h / 80 °C
2.1: triethylamine; diphenyl phosphoryl azide / acetonitrile; 1,4-dioxane / 1 h / 75 °C
2.2: 16 h / 100 °C
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 27 °C
4.1: lithium triethylborohydride / tetrahydrofuran / 1 h / 0 - 27 °C
5.1: hydrogen; palladium 10% on activated carbon / ethanol / 5 h / 20 °C
With
diphenyl phosphoryl azide; palladium 10% on activated carbon; water; hydrogen; lithium triethylborohydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; acetonitrile;
