CarbaMic acid, N-(3-Methylenecyclobutyl)-, phenylMethyl ester

Base Information

Chemical Name:CarbaMic acid, N-(3-Methylenecyclobutyl)-, phenylMethyl ester
CAS No.:130368-98-8
Molecular Formula:C13H15NO2
Molecular Weight:217.268
Hs Code.:
Mol file:130368-98-8.mol

Synonyms:CarbaMic acid, N-(3-Methylenecyclobutyl)-, phenylMethyl ester;(3-Methylenecyclobutyl)-Carbamic Acid Phenylmethyl Ester

Suppliers and Price of CarbaMic acid, N-(3-Methylenecyclobutyl)-, phenylMethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
benzylN-(3-methylidenecyclobutyl)carbamate
100mg
$ 220.00

Crysdot
Benzyl(3-methylenecyclobutyl)carbamate 95+%
1g
$ 446.00

Crysdot
Benzyl(3-methylenecyclobutyl)carbamate 95+%
5g
$ 1340.00

Chemenu
benzyl(3-methylenecyclobutyl)carbamate 95%
5g
$ 1262.00

Chemenu
benzyl(3-methylenecyclobutyl)carbamate 95%
1g
$ 421.00

aablocks
(3-Methylenecyclobutyl)-carbamicacidphenylmethylester 95%
250mg
$ 205.00

Total 9 raw suppliers

Chemical Property of CarbaMic acid, N-(3-Methylenecyclobutyl)-, phenylMethyl ester

Chemical Property:

Boiling Point:358.2±32.0 °C(Predicted)
PKA:12.01±0.20(Predicted)
PSA：38.33000
Density:1.12±0.1 g/cm3(Predicted)
LogP:3.02230

Purity/Quality:

97%, ^*data from raw suppliers

benzylN-(3-methylidenecyclobutyl)carbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of CarbaMic acid, N-(3-Methylenecyclobutyl)-, phenylMethyl ester

There total 5 articles about CarbaMic acid, N-(3-Methylenecyclobutyl)-, phenylMethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 136137-55-8
3-methylenecyclobutan-1-amine hydrochloride

: 501-53-1,94274-21-2
benzyl chloroformate

: 130368-98-8
N-(benzyloxycarbonyl)-3-methylenecyclobutanamine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; Cooling with ice;

Reference yield: 66.3%

: 15760-36-8
3-methylenecyclobutane-1-carboxylic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 130368-98-8
N-(benzyloxycarbonyl)-3-methylenecyclobutanamine

Guidance literature:: 3-methylenecyclobutane-1-carboxylic acid; With diphenyl phosphoryl azide; triethylamine; In 1,4-dioxane; acetonitrile; at 75 ℃; for 1h;

benzyl alcohol; In 1,4-dioxane; acetonitrile; at 100 ℃; for 16h;

Reference yield:

: 15760-35-7
3-methylenecyclobutanecarbonitrile

: 130368-98-8
N-(benzyloxycarbonyl)-3-methylenecyclobutanamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; potassium hydroxide / ethanol / 16 h / 80 °C

2.1: triethylamine; diphenyl phosphoryl azide / acetonitrile; 1,4-dioxane / 1 h / 75 °C

2.2: 16 h / 100 °C

With diphenyl phosphoryl azide; water; triethylamine; potassium hydroxide; In 1,4-dioxane; ethanol; acetonitrile;