Methyl 1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-α-D-fructofuranoside

Base Information

Chemical Name:Methyl 1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-α-D-fructofuranoside
CAS No.:30788-71-7
Molecular Formula:C19H46O6Si4
Molecular Weight:482.913
Hs Code.:
Mol file:30788-71-7.mol

Synonyms:Methyl 1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-α-D-fructofuranoside

Suppliers and Price of Methyl 1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-α-D-fructofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of Methyl 1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-α-D-fructofuranoside

Chemical Property:

Boiling Point:393.6±42.0 °C(Predicted)
PSA：55.38000
Density:0.96±0.1 g/cm3(Predicted)
LogP:4.87110

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methyl 1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-α-D-fructofuranoside

There total 2 articles about Methyl 1-O,3-O,4-O,6-O-tetrakis(trimethylsilyl)-α-D-fructofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25561-30-2
trimethylsilyl 2,2,2-trifluoro-N-(trimethylsilyl)acetimidate

: 13403-14-0,15219-93-9,16975-88-5,51295-55-7,51295-56-8,52443-09-1,60504-77-0,60504-79-2,63526-47-6,69460-17-9,92283-23-3
methyl α-D-fructofuranoside

: 30788-71-7
α-Methyl-fructofuranose-TMS-ether

Guidance literature:: In acetonitrile; at 78 - 80 ℃; for 3h;
DOI:10.1021/jo00381a030

Reference yield:

: 30788-71-7
α-Methyl-fructofuranose-TMS-ether

Guidance literature:: α-Methylfructofuranosid, (CH3)3SiCl / Hexamethyldisilazan;
DOI:10.1016/S0040-4020(01)93099-6

Reference yield:

: 30788-71-7
α-Methyl-fructofuranose-TMS-ether

: 41107-82-8
2,5-anhydro-D-mannitol

Guidance literature:: Multi-step reaction with 2 steps

1: triethylsilane, trimethylsilyl trifluoromethanesulfonate (TMSOTf) / acetonitrile / Ambient temperature

2: water

With triethylsilane; trimethylsilyl trifluoromethanesulfonate; water; In acetonitrile;
DOI:10.1021/jo00381a030