ENAMINE-BB EN300-11723

Base Information

• Chemical Name: ENAMINE-BB EN300-11723
• CAS No.: 10409-15-1
• Molecular Formula: C11H15N
• Molecular Weight: 161.247
• Hs Code.: 2921450090
• Mol file: 10409-15-1.mol

Synonyms:ENAMINE-BB EN300-11723;CHEMBRDG-BB 4011061;N-METHYL-N-1,2,3,4-TETRAHYDRONAPHTHALEN-1-YLAMINE;N-METHYL-1,2,3,4-TETRAHYDRONAPHTHALEN-1-AMINE;N-methyl-1,2,3,4-tetrahydronaphthalen-1-amine(SALTDATA: FREE)

Chemical Property of ENAMINE-BB EN300-11723

Chemical Property:

• Vapor Pressure: 0.0128mmHg at 25°C
• Boiling Point: 259.6°C at 760 mmHg
• Flash Point: 112.7°C
• PSA: 12.03000
• Density: 0.99g/cm³
• LogP: 2.67430

Purity/Quality:

98%,99%, ^*data from raw suppliers

N-Methyl-1,2,3,4-tetrahydronaphthalen-1-amine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn,N
• Statements: 22-36/37/38-51/53
• Safety Statements: 26-61

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ENAMINE-BB EN300-11723

There total 5 articles about ENAMINE-BB EN300-11723 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

N-benzyl-N-methyl-1-amino-1,2,3,4-tetrahydronaphthalene (1010385-40-6) → (-)-N-methyl-1,2,3,4-tetrahydro-1-naphthylamine (10409-15-1) + N-benzyl-1,2,3,4-tetrahydronaphthalen-1-amine (212250-85-6)

Guidance literature:

N-benzyl-N-methyl-1-amino-1,2,3,4-tetrahydronaphthalene; With N-iodo-succinimide; In acetonitrile; at 20 ℃;

With N-methoxylamine hydrochloride; In acetonitrile; at 20 ℃; Further stages.;

DOI:10.1016/j.tetlet.2007.11.162

Reference yield:

N-methyl-3,4-dihydronaphthalen-1(2H )-imine (111865-18-0) → (-)-N-methyl-1,2,3,4-tetrahydro-1-naphthylamine (10409-15-1)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 12h; Inert atmosphere;

DOI:10.1002/anie.201504052

Reference yield:

1-tetralone oxime (3349-64-2,68253-36-1,100485-58-3) → (-)-N-methyl-1,2,3,4-tetrahydro-1-naphthylamine (10409-15-1)

Guidance literature:

Multi-step reaction with 2 steps

1: Na, EtOH

2: (i) Et₃N, dioxane, (ii) LiAlH₄, Et₂O

With ethanol; sodium;

upstream raw materials:

1,2,3,4-tetrahydronaphthalen-1-amine

chloroformic acid ethyl ester

1-tetralone oxime

N-benzyl-N-methyl-1-amino-1,2,3,4-tetrahydronaphthalene

Downstream raw materials:

(S)-N-methyl-1,2,3,4-tetrahydro-1-naphthylamine (-)-dibenzoyltartrate

(R)-N-methyl-1,2,3,4-tetrahydro-1-naphthylamine (+)-dibenzoyltartrate

(+/-)[6-(2,6-diethyl-phenyl)-4-methoxy-2-methyl-pyridin-3-ylmethyl]-methyl-(1,2,3,4-tetrahydro-naphthalen-1-yl)-amine

3,4-dihydronaphthalene-1(2H)-one

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