O-(2-Nitrobenzyl)-L-tyrosine Hydrochloride

Base Information

• Chemical Name: O-(2-Nitrobenzyl)-L-tyrosine Hydrochloride
• CAS No.: 207727-86-4
• Molecular Formula: C16H17ClN2O5
• Molecular Weight: 352.76958
• Hs Code.: 2904909090
• Mol file: 207727-86-4.mol

Synonyms:O-(2-Nitrobenzyl)-L-tyrosine Hydrochloride;(S)-2-amino-3-(4-(2-nitrobenzyloxy)phenyl)propanoic acid hydrochloride;O-[(2-Nitrophenyl)Methyl]-L-tyrosine Hydrochloride;o-nitrobenzyl-O-tyrosine.HCl

Chemical Property of O-(2-Nitrobenzyl)-L-tyrosine Hydrochloride

Chemical Property:

• PSA: 118.37000
• LogP: 4.15370
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

O-(2-Nitrobenzyl)-L-tyrosine hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: A novel derivative of Tyrosine, O-(2-Nitrobenzyl)-L-tyrosine Hydrochloride can be used in the synthesis of caged peptides. A novel derivative of Tyrosine used in the synthesis of caged peptides. L-Tyrosine caged with photosensitive ortho-nitrobenzyl side chain

Technology Process of O-(2-Nitrobenzyl)-L-tyrosine Hydrochloride

There total 5 articles about O-(2-Nitrobenzyl)-L-tyrosine Hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-nitrobenzyl chloride (612-23-7) + L-tyrosine (60-18-4,18875-48-4,25619-78-7,30704-25-7) → O-(2-nitrobenzyl)-L-tyrosine hydrochloride (207727-86-4)

Guidance literature:

L-tyrosine; With sodium hydroxide; copper(II) sulfate; In water; at 23 ℃;

2-nitrobenzyl chloride; With sodium hydroxide; In methanol; water; N,N-dimethyl-formamide; at 23 ℃;

With hydrogenchloride; In water; at 23 ℃;

DOI:10.1021/ja801602q

Reference yield:

C30H26CuN4O10 → O-(2-nitrobenzyl)-L-tyrosine hydrochloride (207727-86-4)

Guidance literature:

With hydrogenchloride; In water; at 20 ℃; for 1h; Darkness;

DOI:10.1016/j.tetlet.2017.08.034

Reference yield:

L-tyrosine (60-18-4,18875-48-4,25619-78-7,30704-25-7) → O-(2-nitrobenzyl)-L-tyrosine hydrochloride (207727-86-4)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / water / 1.5 h / 20 °C

2: potassium carbonate / water; N,N-dimethyl-formamide / 24 h / 20 °C

3: hydrogenchloride / water / 1 h

With hydrogenchloride; potassium carbonate; sodium hydroxide; In water; N,N-dimethyl-formamide;

DOI:10.1021/jacs.5b12680

upstream raw materials:

2-nitrobenzyl chloride

L-tyrosine

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