3,3-DIMETHYL-13-(4-NITRO-PHENYL)-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE

Base Information

Chemical Name:3,3-DIMETHYL-13-(4-NITRO-PHENYL)-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE
CAS No.:1017238-97-9
Molecular Formula:C23H19N3O5
Molecular Weight:417.421
Hs Code.:
Mol file:1017238-97-9.mol

Synonyms:3,3-DIMETHYL-13-(4-NITRO-PHENYL)-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE;3,3-Dimethyl-13-(4-nitrophenyl)-2,3,4,13-tetrahydroindazolo[1,2-b]phthalazine-1,6,11-trio

Suppliers and Price of 3,3-DIMETHYL-13-(4-NITRO-PHENYL)-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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American Custom Chemicals Corporation
3,3-DIMETHYL-13-(4-NITRO-PHENYL)-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE 95.00%
1G
$ 1273.39

Total 0 raw suppliers

Chemical Property of 3,3-DIMETHYL-13-(4-NITRO-PHENYL)-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE

Chemical Property:

PSA：106.89000
LogP:3.79780

Purity/Quality:: 3,3-DIMETHYL-13-(4-NITRO-PHENYL)-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,3-DIMETHYL-13-(4-NITRO-PHENYL)-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE

There total 12 articles about 3,3-DIMETHYL-13-(4-NITRO-PHENYL)-2,3,4,13-TETRAHYDRO-INDAZOLO[1,2-B]PHTHALAZINE-1,6,11-TRIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 85-44-9
phthalic anhydride

: 555-16-8
4-nitrobenzaldehdye

: 126-81-8
dimedone

: 1017238-97-9
3,3-dimethyl-13-(4-nitrophenyl)-3,4-dihydro-2H-indazolo[1,2-b]phthalazine-1,6,11(13H)-trione

Guidance literature:: With hydrazine hydrate; In neat (no solvent); at 80 ℃; for 0.333333h;
DOI:10.1039/c6ra06376d

Reference yield: 96.0%

: 1445-69-8
2,3-dihydrophthalazine-1,4-dione

: 3471-13-4
dimedone

: 555-16-8
4-nitrobenzaldehdye

: 1017238-97-9
3,3-dimethyl-13-(4-nitrophenyl)-3,4-dihydro-2H-indazolo[1,2-b]phthalazine-1,6,11(13H)-trione

Guidance literature:: With SBA-15 sulfonic acid mesoporous silicas; In acetonitrile; at 45 ℃; for 0.3h; Irradiation; Green chemistry;
DOI:10.1016/j.molcata.2013.03.017