μ-Benzenebis[N,N'-(1,3-dimethyl-1,3-propanediylidene)bis(2,6-dichlorobenzenaminato)]dicopper(I),benzeneadduct,min.98%

Base Information

• Chemical Name: μ-Benzenebis[N,N'-(1,3-dimethyl-1,3-propanediylidene)bis(2,6-dichlorobenzenaminato)]dicopper(I),benzeneadduct,min.98%
• CAS No.: 1119821-62-3
• Molecular Formula: C40H28Cl8Cu2N4++
• Molecular Weight: 1047.54696
• Mol file: 1119821-62-3.mol

Synonyms:μ-Benzenebis[N,N'-(1,3-dimethyl-1,3-propanediylidene)bis(2,6-dichlorobenzenaminato)]dicopper(I),benzeneadduct,min.98%

Chemical Property of μ-Benzenebis[N,N'-(1,3-dimethyl-1,3-propanediylidene)bis(2,6-dichlorobenzenaminato)]dicopper(I),benzeneadduct,min.98%

Chemical Property:

• PSA: 12.50000
• LogP: 14.41820
• Sensitive.: air sensitive, moisture sensitiv

Purity/Quality:

98%...99.99%. ^*data from raw suppliers

μ-Benzenebis[N,N'-(1,3-dimethyl-1,3-propanediylidene)bis(2,6-dichlorobenzenaminato)] dicopper(I), benzene adduct, min. 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 1. High yield C-H amination of unactivated C-H bonds with 1-adamantylazide.

Technology Process of μ-Benzenebis[N,N'-(1,3-dimethyl-1,3-propanediylidene)bis(2,6-dichlorobenzenaminato)]dicopper(I),benzeneadduct,min.98%

There total 1 articles about μ-Benzenebis[N,N'-(1,3-dimethyl-1,3-propanediylidene)bis(2,6-dichlorobenzenaminato)]dicopper(I),benzeneadduct,min.98% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

H(Cl2C6H3)2N2CCH3CHCCH3 (445460-78-6) + copper (I) tert-butoxide (35342-67-7,35342-68-8) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → [(copper)CH(C(CH3)NC6H3Cl2)2]2(μ-benzene) (1119821-62-3)

Guidance literature:

In benzene; according to P.H.M. Budzelaar, N.N.P. Moonen, R. de Gelder, J.M.M.Smits,A.W. Gal, Chem. Eur. J. 2000, 6, 2740;

DOI:10.1002/anie.200804304

Reference yield: 63.0%

1-Azidoadamantane (24886-73-5) + [(copper)CH(C(CH3)NC6H3Cl2)2]2(μ-benzene) (1119821-62-3) → (μ-Nadamantyl)((copper)CH(C(CH3)NC6H3Cl2)2)2

Guidance literature:

In chlorobenzene; byproducts: N2;

DOI:10.1002/anie.200804304

Reference yield:

{[Cl2NN]Cu}2(benzene) (1119821-62-3) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → [Cl2NN]Cu(benzene) (1215208-99-3)

Guidance literature:

upstream raw materials:

H(Cl₂C₆H₃)2N₂CCH₃CHCCH₃

copper (I) tert-butoxide

benzene

Downstream raw materials:

[Cl₂NN]Cu(benzene)

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