3-CHLORO-4-IODOPHENOL

Base Information

• Chemical Name: 3-CHLORO-4-IODOPHENOL
• CAS No.: 855403-42-8
• Molecular Formula: C6H4ClIO
• Molecular Weight: 254.455
• Hs Code.: 2908199090
• Mol file: 855403-42-8.mol

Synonyms:3-CHLORO-4-IODOPHENOL;Phenol, 3-chloro-4-iodo-

Chemical Property of 3-CHLORO-4-IODOPHENOL

Chemical Property:

• Melting Point: 40 °C
• Boiling Point: 296.9±25.0 °C(Predicted)
• PKA: 8.39±0.18(Predicted)
• PSA: 20.23000
• Density: 2.087±0.06 g/cm3(Predicted)
• LogP: 2.65020
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

99%, ^*data from raw suppliers

3-Chloro-4-iodophenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-CHLORO-4-IODOPHENOL

There total 4 articles about 3-CHLORO-4-IODOPHENOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-chloro-4-nitrosophenol (40140-91-8) → m-chloro-p-iodophenol (855403-42-8)

Guidance literature:

With hydrogen bromide; potassium iodide; at 70 - 80 ℃;

Reference yield:

2,4-dichloro-1-iodo-benzene (29898-32-6) + sodium methylate (124-41-4) → m-chloro-p-iodophenol (855403-42-8)

Guidance literature:

With methanol; at 183 ℃;

Reference yield:

3-monochlorophenol (108-43-0) → m-chloro-p-iodophenol (855403-42-8)

Guidance literature:

With perchloric acid; sodium perchlorate; Iodine monochloride; sodium chloride; In acetic acid; at 35 ℃; Kinetics; Mechanism; effect of HClO₄ concentration;

upstream raw materials:

2,4-dichloro-1-iodo-benzene

sodium methylate

3-monochlorophenol

3-chloro-4-nitrosophenol

Refernces

• 1、 Prasada Rao, M. D.,Padmanabha, J.. "Kinetics and Mechanism of Iodination of Phenol and Substituted Phenols by Iodine Monochloride in Aqueous Acetic Acid". . p. 133 - 135. Retrieved 2007/10/02.