3,5-dichloro-4-(hydroxyMethyl)phenol

Base Information

• Chemical Name: 3,5-dichloro-4-(hydroxyMethyl)phenol
• CAS No.: 720679-54-9
• Molecular Formula: C7H6Cl2O2
• Molecular Weight: 193.029
• Hs Code.: 2908199090
• Mol file: 720679-54-9.mol

Synonyms:3,5-dichloro-4-(hydroxyMethyl)phenol;2,6-Dichloro-4-hydroxybenzenemethanol;4-Hydroxymethyl-3,5-dichlorophenol

Chemical Property of 3,5-dichloro-4-(hydroxyMethyl)phenol

Chemical Property:

• PSA: 40.46000
• LogP: 2.19130
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

3,5-Dichloro-4-(hydroxymethyl)phenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3,5-Dichloro-4-(hydroxymethyl)phenol can be used for their insecticidal and acaricidal properties.

Technology Process of 3,5-dichloro-4-(hydroxyMethyl)phenol

There total 2 articles about 3,5-dichloro-4-(hydroxyMethyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2,6-dichloro-4-hydroxybenzaldehyde (60964-09-2) → 3,5-dichloro-4-(hydroxymethyl)phenol (720679-54-9)

Guidance literature:

With sodium tetrahydroborate; water; In ethanol; for 1h;

DOI:10.1002/cmdc.201300015

Reference yield: 66.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 3,5-dichlorophenol (591-35-5) → 3,5-dichloro-4-(hydroxymethyl)phenol (720679-54-9)

Guidance literature:

With sodium metaborate tetrahydrate; In water; at 50 ℃;

DOI:10.1021/acs.orglett.9b02372

Reference yield: 95.0%

dichloroacethyl chloride (79-36-7) + 3,5-dichloro-4-(hydroxymethyl)phenol (720679-54-9) → 3,5-dichloro-4-((2,2-dichloroacetoxy)methyl)phenyl 2,2-dichloroacetate

Guidance literature:

3,5-dichloro-4-(hydroxymethyl)phenol; With pyridine; In dichloromethane; at 0 ℃; for 0.0833333h;

dichloroacethyl chloride; In dichloromethane; at 20 ℃; for 0.333333h;

DOI:10.1021/acs.orglett.9b02372

upstream raw materials:

formaldehyd

3,5-dichlorophenol

2,6-dichloro-4-hydroxybenzaldehyde

Downstream raw materials:

[2,6-dichloro-4-(3,3-dichloro-allyloxy)-phenyl]-methanol

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