benzyl (4,5,7,8-tetrahydro-4-oxo-3H-pyrano[4,3-d]pyrimidin-2-yl)methylcarbamate

Base Information

• Chemical Name: benzyl (4,5,7,8-tetrahydro-4-oxo-3H-pyrano[4,3-d]pyrimidin-2-yl)methylcarbamate
• CAS No.: 1418131-84-6
• Molecular Formula: C₁₆H₁₇N₃O₄
• Molecular Weight: 315.329
• Mol file: 1418131-84-6.mol

Synonyms:benzyl (4,5,7,8-tetrahydro-4-oxo-3H-pyrano[4,3-d]pyrimidin-2-yl)methylcarbamate

Chemical Property of benzyl (4,5,7,8-tetrahydro-4-oxo-3H-pyrano[4,3-d]pyrimidin-2-yl)methylcarbamate

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

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Technology Process of benzyl (4,5,7,8-tetrahydro-4-oxo-3H-pyrano[4,3-d]pyrimidin-2-yl)methylcarbamate

There total 6 articles about benzyl (4,5,7,8-tetrahydro-4-oxo-3H-pyrano[4,3-d]pyrimidin-2-yl)methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

benzyl 2-amino-2-iminoethylcarbamate hydrochloride + 4-oxotetrahydro-2H-pyran-3-carboxylic acid methyl ester (127956-11-0) → benzyl [(4-oxo-4,5,7,8-tetrahydro-3H-pyrano[4,3-d]pyrimidin-2-yl)methyl]carbamate (1418131-84-6)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 15h; Reagent/catalyst; Temperature; Solvent;

Reference yield: 55.0%

2-<(phenylmethoxy)carbonyl>aminoacetamidine (77390-81-9) + 4-oxotetrahydro-2H-pyran-3-carboxylic acid methyl ester (127956-11-0) → benzyl [(4-oxo-4,5,7,8-tetrahydro-3H-pyrano[4,3-d]pyrimidin-2-yl)methyl]carbamate (1418131-84-6)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 15h;

Reference yield: 55.0%

2-<(phenylmethoxy)carbonyl>aminoacetamidine hydrochloride (50850-19-6) + 4-oxotetrahydro-2H-pyran-3-carboxylic acid methyl ester (127956-11-0) → benzyl [(4-oxo-4,5,7,8-tetrahydro-3H-pyrano[4,3-d]pyrimidin-2-yl)methyl]carbamate (1418131-84-6)

Guidance literature:

With sodium ethanolate; In ethanol; for 24h; Reflux;

upstream raw materials:

methyl 2-(((benzyloxy)carbonyl)amino)acetimidate

2-<(phenylmethoxy)carbonyl>aminoacetamidine

4-oxotetrahydro-2H-pyran-3-carboxylic acid methyl ester

Tetrahydro-4H-pyran-4-one

Downstream raw materials:

N-((4-oxo-4,5,7,8-tetrahydro-3H-pyrano[4,3-d]pyrimidin-2-yl)methyl)-3-phenyl-N-(thiophen-2-ylmethyl)propanamide

C₂₃H₂₉N₃O₃

C₁₉H₂₃N₃O₄

2-(4-(4-fluorobenzoyl)piperidin-1-yl)-N-((4-oxo-4,5,7,8-tetrahydro-3H-pyrano[4,3-d]pyrimidin-2-yl)methyl)acetamide

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